3-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-5-(hydroxymethyl)benzonitrile

Base Information

Chemical Name:3-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-5-(hydroxymethyl)benzonitrile
CAS No.:171082-06-7
Molecular Formula:C₃₀H₂₇NO₄
Molecular Weight:465.549
Hs Code.:

Synonyms:3-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-5-(hydroxymethyl)benzonitrile

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Chemical Property of 3-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-5-(hydroxymethyl)benzonitrile

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Technology Process of 3-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-5-(hydroxymethyl)benzonitrile

There total 7 articles about 3-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-5-(hydroxymethyl)benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.3%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 146335-23-1
3,5-bis(hydroxymethyl)benzonitrile

: 171082-06-7
3-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-5-(hydroxymethyl)benzonitrile

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1080/15257779908043075

Reference yield:

: 618-88-2
5-nitrobenzene-1,3-dicarboxylic acid

: 171082-06-7
3-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-5-(hydroxymethyl)benzonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / H₂ / Pd/C / methanol / 1 h / 20 °C / 760 Torr

2: 82 percent / conc. H₂SO₄ / 16 h / Heating

3: 82 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

4: 1.) aq. NaNO₂, aq. HCl / 1.) -5 deg C, 30 min, 2.) H₂O, 0 deg C, 2 h

5: 52.3 percent / pyridine / 20 °C

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; sulfuric acid; hydrogen; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1080/15257779908043075

Reference yield:

: 99-27-4
dimethyl 5-aminoisophthalate

: 171082-06-7
3-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-5-(hydroxymethyl)benzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux

2.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 - 5 °C

2.2: 20 °C

3.1: pyridine / 20 °C

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; sodium nitrite; In tetrahydrofuran; water;