benzyl N-{3-[N-methyl(4-{[(tert-butoxy)carbonyl]amino}benzene)amido]phenyl}carbamate

Base Information

Chemical Name:benzyl N-{3-[N-methyl(4-{[(tert-butoxy)carbonyl]amino}benzene)amido]phenyl}carbamate
CAS No.:1604811-88-2
Molecular Formula:C₂₇H₂₉N₃O₅
Molecular Weight:475.544
Hs Code.:

Synonyms:benzyl N-{3-[N-methyl(4-{[(tert-butoxy)carbonyl]amino}benzene)amido]phenyl}carbamate

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Chemical Property of benzyl N-{3-[N-methyl(4-{[(tert-butoxy)carbonyl]amino}benzene)amido]phenyl}carbamate

Chemical Property:

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Technology Process of benzyl N-{3-[N-methyl(4-{[(tert-butoxy)carbonyl]amino}benzene)amido]phenyl}carbamate

There total 6 articles about benzyl N-{3-[N-methyl(4-{[(tert-butoxy)carbonyl]amino}benzene)amido]phenyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 66493-39-8
4-(N-tert-butoxycarbonyl)aminobenzoic acid

: 1604811-85-9
benzyl 3-(methylamino)phenylcarbamate

: 1604811-88-2
benzyl N-{3-[N-methyl(4-{[(tert-butoxy)carbonyl]amino}benzene)amido]phenyl}carbamate

Guidance literature:: With 2-(Dimethylamino)pyridine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 113261-00-0
benzyl (3-aminophenyl)carbamate

: 1604811-88-2
benzyl N-{3-[N-methyl(4-{[(tert-butoxy)carbonyl]amino}benzene)amido]phenyl}carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / dichloromethane / 20 °C

2.1: lithium aluminium tetrahydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 - 20 °C

2.2: 4 h / 20 °C

3.1: methanol; sodium hydroxide / tetrahydrofuran / 4 h / 20 °C

4.1: 2-(Dimethylamino)pyridine / dichloromethane; N,N-dimethyl-formamide / 20 °C

With pyridine; methanol; 2-(Dimethylamino)pyridine; lithium aluminium tetrahydride; sodium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1604811-88-2
benzyl N-{3-[N-methyl(4-{[(tert-butoxy)carbonyl]amino}benzene)amido]phenyl}carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C

2.1: pyridine / dichloromethane / 20 °C

3.1: lithium aluminium tetrahydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 - 20 °C

3.2: 4 h / 20 °C

4.1: methanol; sodium hydroxide / tetrahydrofuran / 4 h / 20 °C

5.1: 2-(Dimethylamino)pyridine / dichloromethane; N,N-dimethyl-formamide / 20 °C

With pyridine; methanol; 2-(Dimethylamino)pyridine; lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;