acetic acid 3-{4-[5-(3-acetoxy-propyl)-3-chloro-2-methoxymethoxy-phenoxy]-3-bromo-5-chloro-phenyl}-propyl ester

Base Information

Chemical Name:acetic acid 3-{4-[5-(3-acetoxy-propyl)-3-chloro-2-methoxymethoxy-phenoxy]-3-bromo-5-chloro-phenyl}-propyl ester
CAS No.:704912-99-2
Molecular Formula:C₂₄H₂₇BrCl₂O₇
Molecular Weight:578.284
Hs Code.:

Synonyms:acetic acid 3-{4-[5-(3-acetoxy-propyl)-3-chloro-2-methoxymethoxy-phenoxy]-3-bromo-5-chloro-phenyl}-propyl ester

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Chemical Property of acetic acid 3-{4-[5-(3-acetoxy-propyl)-3-chloro-2-methoxymethoxy-phenoxy]-3-bromo-5-chloro-phenyl}-propyl ester

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Technology Process of acetic acid 3-{4-[5-(3-acetoxy-propyl)-3-chloro-2-methoxymethoxy-phenoxy]-3-bromo-5-chloro-phenyl}-propyl ester

There total 5 articles about acetic acid 3-{4-[5-(3-acetoxy-propyl)-3-chloro-2-methoxymethoxy-phenoxy]-3-bromo-5-chloro-phenyl}-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 107-30-2
chloromethyl methyl ether

: 704912-91-4
3-[5-(4-(3-acetyloxypropyl)-2-bromo-6-chlorophenoxy)-3-chloro-4-hydroxyphenyl]propyl acetate

: 704912-99-2
acetic acid 3-{4-[5-(3-acetoxy-propyl)-3-chloro-2-methoxymethoxy-phenoxy]-3-bromo-5-chloro-phenyl}-propyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/j.bmc.2005.11.055

Reference yield:

: 80373-18-8
3-(4'-hydroxyphenyl)-1-propyl acetate

: 704912-99-2
acetic acid 3-{4-[5-(3-acetoxy-propyl)-3-chloro-2-methoxymethoxy-phenoxy]-3-bromo-5-chloro-phenyl}-propyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 64 percent / SO₂Cl₂ / 5 h / 0 °C

2: 100 percent / pyridine*HBr₃; pyridine / CHCl₃ / 3 h / 0 °C

3: 50 percent / LiClO₄ / Electrochemical reaction

4: 70 percent / Zn; AcOH / tetrahydrofuran / 0 °C

5: 100 percent / DIPEA / CH₂Cl₂

With pyridine; sulfuryl dichloride; pyridinium perbromide hydrobromide; lithium perchlorate; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; In tetrahydrofuran; dichloromethane; chloroform;
DOI:10.1016/j.bmc.2005.11.055

Reference yield:

: 704912-87-8
3-(5-bromo-3-chloro-4-hydroxyphenyl)propyl acetate

: 704912-99-2
acetic acid 3-{4-[5-(3-acetoxy-propyl)-3-chloro-2-methoxymethoxy-phenoxy]-3-bromo-5-chloro-phenyl}-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / LiClO₄ / Electrochemical reaction

2: 70 percent / Zn; AcOH / tetrahydrofuran / 0 °C

3: 100 percent / DIPEA / CH₂Cl₂

With lithium perchlorate; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmc.2005.11.055