D-[2-13C]TALOSE

Base Information

• Chemical Name: D-[2-13C]TALOSE
• CAS No.: 83379-36-6
• Molecular Formula: C₆H₁₂O₆
• Molecular Weight: 181.147
• Mol file: 83379-36-6.mol

Synonyms:<1-13C>-D-threose;D-[1-13C]mannose;C2-13C-D-glucose;D-[2-13C]glucose;D-<1-13C>threose;<1-13C>-D-mannose;[2-13C]glucose;2-(13)C-D-glucose;

Chemical Property of D-[2-13C]TALOSE

Chemical Property:

• PSA: 110.38000
• LogP: -3.22140

Purity/Quality:

99% ^*data from raw suppliers

D-Talose-2-13C ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of D-[2-13C]TALOSE

There total 1 articles about D-[2-13C]TALOSE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

<1-13C>-D-mannose (70849-31-9,478519-02-7) → [1-13C]D-glucose (40762-22-9,478519-02-7) + D-<2-13C>glucose (70849-16-0,83379-35-5,83379-36-6,70849-17-1,478529-73-6)

Guidance literature:

molybdenum(VI) oxide; In water; at 92 ℃;

DOI:10.1016/S0008-6215(00)90268-4

Reference yield: 60.0%

benzyl bromide (100-39-0) + D-<2-13C>glucose (70849-16-0,83379-35-5,83379-36-6,70849-17-1,478529-73-6) → C2-13C-tri-O-benzyl-D-glucal (444313-78-4)

Guidance literature:

Multistep reaction.;

DOI:10.1021/ja026281n

Reference yield:

D-<2-13C>glucose (70849-16-0,83379-35-5,83379-36-6,70849-17-1,478529-73-6) → glycolic Acid (79-14-1) + D-glyceric acid (473-81-4,600-19-1,6000-40-4,28305-26-2,118916-26-0) + C(13)CH2O4 (276672-31-2) + C4(13)CH8O7

Guidance literature:

With sodium hydroxide; sulfuric acid; ozone; In water; at 20 ℃; pH=2.5;

DOI:10.1016/j.carres.2009.05.012

upstream raw materials:

<1-13C>-D-mannose

Downstream raw materials:

C₂-¹³C-tri-O-benzyl-D-glucal

glycolic Acid

D-glyceric acid

C⁽¹³⁾CH₂O₄