N-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

Base Information

Chemical Name:N-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide
CAS No.:218628-43-4
Molecular Formula:C₃₁H₃₁NO₆Se
Molecular Weight:592.55
Hs Code.:

Synonyms:N-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

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Chemical Property of N-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

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Technology Process of N-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

There total 7 articles about N-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 5707-04-0
Phenylselenyl chloride

: 218628-42-3
N-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)acetamide

: 218628-43-4
N-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃;
DOI:10.1055/s-1998-1937

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 218628-43-4
N-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzene / 2 h / Heating

2.1: pyridine / benzene / 2 h / 30 - 40 °C

3.1: LDA / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 0.75 h / -78 °C

3.2: 65 percent / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 1 h / -78 °C

With pyridine; lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; benzene; 1.1: Condensation / 2.1: Acylation / 3.1: Metallation / 3.2: Substitution;
DOI:10.1039/a900467j

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 218628-43-4
N-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzene / 2 h / Heating

2.1: pyridine / benzene / 2 h / 30 - 40 °C

3.1: LDA / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 0.75 h / -78 °C

3.2: 65 percent / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 1 h / -78 °C

With pyridine; lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; benzene; 1.1: Condensation / 2.1: Acylation / 3.1: Metallation / 3.2: Substitution;
DOI:10.1039/a900467j