Technology Process of C38H35NO5
There total 9 articles about C38H35NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C41H39NO5;
With
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; methanol;
for 0.166667h;
Inert atmosphere;
With
potassium carbonate;
In
tetrahydrofuran; methanol;
at 68 ℃;
for 3h;
Inert atmosphere;
DOI:10.1002/ejoc.201300072
- Guidance literature:
-
N-[2,4-bis(benzyloxy)phenethyl]-2-(4-allyloxyphenyl)acetamide;
With
trichlorophosphate;
In
chloroform;
for 17h;
Reflux;
With
[(1S,2S)-N-(p-toluensulfonyl)-1,2-diphenylethanediamine](p-cymene)ruthenium (I); formic acid; triethylamine;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 20h;
Inert atmosphere;
benzyl chloroformate;
Further stages;
DOI:10.3390/molecules22091450
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: chloro {[(1S,2S)-(+)-2-amino-1,2-diphenylethyl]((4-toluenesulfonyl)amido)(p-cymene)}ruthenium(ll); / N,N-dimethyl-formamide / 2 h / 0 - 20 °C
2.1: triethylamine; dmap / dichloromethane / 1.5 h / 10 - 50 °C
3.1: tetrakis(triphenylphosphine) palladium(0) / methanol; tetrahydrofuran / 0.17 h / Inert atmosphere
3.2: 3 h / 68 °C / Inert atmosphere
With
dmap; tetrakis(triphenylphosphine) palladium(0); chloro {[(1S,2S)-(+)-2-amino-1,2-diphenylethyl]((4-toluenesulfonyl)amido)(p-cymene)}ruthenium(ll); triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201300072