1,1-dimethylethyl 3-bromo-1-methyl-5-(phenylmethoxy)-1H-indole-2-carboxylate

Base Information

Chemical Name:1,1-dimethylethyl 3-bromo-1-methyl-5-(phenylmethoxy)-1H-indole-2-carboxylate
CAS No.:167380-81-6
Molecular Formula:C₂₁H₂₂BrNO₃
Molecular Weight:416.315
Hs Code.:

Synonyms:1,1-dimethylethyl 3-bromo-1-methyl-5-(phenylmethoxy)-1H-indole-2-carboxylate

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Chemical Property of 1,1-dimethylethyl 3-bromo-1-methyl-5-(phenylmethoxy)-1H-indole-2-carboxylate

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Technology Process of 1,1-dimethylethyl 3-bromo-1-methyl-5-(phenylmethoxy)-1H-indole-2-carboxylate

There total 3 articles about 1,1-dimethylethyl 3-bromo-1-methyl-5-(phenylmethoxy)-1H-indole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 167380-80-5
3-bromo-1-methyl-5-(phenylmethoxy)-1H-indole-2-carboxylic acid

: 36805-97-7
N,N-dimethylformamide di-tert-butyl acetal

: 167380-81-6
1,1-dimethylethyl 3-bromo-1-methyl-5-(phenylmethoxy)-1H-indole-2-carboxylate

Guidance literature:: In toluene; for 2h; Heating;
DOI:10.1002/jhet.5570330614

Reference yield:

: 61905-91-7
ethyl 1-methyl-5-(phenylmethoxy)-1H-indole-2-carboxylate

: 167380-81-6
1,1-dimethylethyl 3-bromo-1-methyl-5-(phenylmethoxy)-1H-indole-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / pyridine, pyridinium bromide perbromide / 16 h

2: 96 percent / KOH / methanol; H₂O / 5 h / Heating

3: 74 percent / toluene / 2 h / Heating

With pyridine; potassium hydroxide; pyridinium hydrobromide perbromide; In methanol; water; toluene;
DOI:10.1002/jhet.5570330614

Reference yield:

: 167380-79-2
ethyl 3-bromo-1-methyl-5-(phenylmethoxy)-1H-indole-2-carboxylate

: 167380-81-6
1,1-dimethylethyl 3-bromo-1-methyl-5-(phenylmethoxy)-1H-indole-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / KOH / methanol; H₂O / 5 h / Heating

2: 74 percent / toluene / 2 h / Heating

With potassium hydroxide; In methanol; water; toluene;
DOI:10.1002/jhet.5570330614