(2S,2'S)-tetra-tert-butyl 2,2'-((5-nitroisophthaloyl)bis(azanediyl))disuccinate

Base Information

Chemical Name:(2S,2'S)-tetra-tert-butyl 2,2'-((5-nitroisophthaloyl)bis(azanediyl))disuccinate
CAS No.:1262887-73-9
Molecular Formula:C₃₂H₄₇N₃O₁₂
Molecular Weight:665.738
Hs Code.:

Synonyms:(2S,2'S)-tetra-tert-butyl 2,2'-((5-nitroisophthaloyl)bis(azanediyl))disuccinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,2'S)-tetra-tert-butyl 2,2'-((5-nitroisophthaloyl)bis(azanediyl))disuccinate

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Technology Process of (2S,2'S)-tetra-tert-butyl 2,2'-((5-nitroisophthaloyl)bis(azanediyl))disuccinate

There total 1 articles about (2S,2'S)-tetra-tert-butyl 2,2'-((5-nitroisophthaloyl)bis(azanediyl))disuccinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 13438-30-7
5-nitro-1,3-benzenedicarbonylchloride

: 1791-13-5,135904-71-1
L-aspartic acid di-tert-butyl ester hydrochloride

: 1262887-73-9
(2S,2'S)-tetra-tert-butyl 2,2'-((5-nitroisophthaloyl)bis(azanediyl))disuccinate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c0cc04754f

Reference yield: 87.0%

: 1262887-73-9
(2S,2'S)-tetra-tert-butyl 2,2'-((5-nitroisophthaloyl)bis(azanediyl))disuccinate

: 1262887-74-0
(2S,2'S)-tetra-tert-butyl 2,2'-((5-aminoisophthaloyl)bis(azanediyl))disuccinate

Guidance literature:: With 10% palladium on activated carbon; hydrogen; In methanol;
DOI:10.1039/c0cc04754f

Reference yield:

: 1262887-73-9
(2S,2'S)-tetra-tert-butyl 2,2'-((5-nitroisophthaloyl)bis(azanediyl))disuccinate

: 1262887-75-1
(2S,2'S)-tetra-tert-butyl 2,2'-((5-([2,2'-bipyridine]-5-carboxamido)isophthaloyl)bis(azanediyl))disuccinate

Guidance literature:: Multi-step reaction with 2 steps

1: 10% palladium on activated carbon; hydrogen / methanol

2: triethylamine / chloroform / 18 h / Reflux; Inert atmosphere

With 10% palladium on activated carbon; hydrogen; triethylamine; In methanol; chloroform;
DOI:10.1039/c0cc04754f