(2S,2'S)-tetra-tert-butyl 2,2'-((5-aminoisophthaloyl)bis(azanediyl))disuccinate

Base Information

Chemical Name:(2S,2'S)-tetra-tert-butyl 2,2'-((5-aminoisophthaloyl)bis(azanediyl))disuccinate
CAS No.:1262887-74-0
Molecular Formula:C₃₂H₄₉N₃O₁₀
Molecular Weight:635.755
Hs Code.:

Synonyms:(2S,2'S)-tetra-tert-butyl 2,2'-((5-aminoisophthaloyl)bis(azanediyl))disuccinate

Suppliers and Price of (2S,2'S)-tetra-tert-butyl 2,2'-((5-aminoisophthaloyl)bis(azanediyl))disuccinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,2'S)-tetra-tert-butyl 2,2'-((5-aminoisophthaloyl)bis(azanediyl))disuccinate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,2'S)-tetra-tert-butyl 2,2'-((5-aminoisophthaloyl)bis(azanediyl))disuccinate

There total 3 articles about (2S,2'S)-tetra-tert-butyl 2,2'-((5-aminoisophthaloyl)bis(azanediyl))disuccinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1262887-73-9
(2S,2'S)-tetra-tert-butyl 2,2'-((5-nitroisophthaloyl)bis(azanediyl))disuccinate

: 1262887-74-0
(2S,2'S)-tetra-tert-butyl 2,2'-((5-aminoisophthaloyl)bis(azanediyl))disuccinate

Guidance literature:: With 10% palladium on activated carbon; hydrogen; In methanol;
DOI:10.1039/c0cc04754f

Reference yield:

: 13438-30-7
5-nitro-1,3-benzenedicarbonylchloride

: 1262887-74-0
(2S,2'S)-tetra-tert-butyl 2,2'-((5-aminoisophthaloyl)bis(azanediyl))disuccinate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: 10% palladium on activated carbon; hydrogen / methanol

With 10% palladium on activated carbon; hydrogen; triethylamine; In methanol; dichloromethane;
DOI:10.1039/c0cc04754f

Reference yield:

: 1791-13-5,135904-71-1
L-aspartic acid di-tert-butyl ester hydrochloride

: 1262887-74-0
(2S,2'S)-tetra-tert-butyl 2,2'-((5-aminoisophthaloyl)bis(azanediyl))disuccinate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: 10% palladium on activated carbon; hydrogen / methanol

With 10% palladium on activated carbon; hydrogen; triethylamine; In methanol; dichloromethane;
DOI:10.1039/c0cc04754f