3-Hydrazinylbenzenesulfonamide hydrochloride

Base Information

• Chemical Name: 3-Hydrazinylbenzenesulfonamide hydrochloride
• CAS No.: 131774-72-6
• Molecular Formula: C6H9N3O2S
• Molecular Weight: 187.222
• Hs Code.: 2935009090
• European Community (EC) Number: 690-949-2
• DSSTox Substance ID: DTXSID30696036
• Mol file: 131774-72-6.mol

Synonyms:1220039-75-7;3-hydrazinylbenzenesulfonamide hydrochloride;3-HYDRAZINO-BENZENESULFONAMIDE HYDROCHLORIDE;3-hydrazinylbenzene-1-sulfonamide hydrochloride;3-hydrazinylbenzenesulfonamide;hydrochloride;SCHEMBL11777840;DTXSID30696036;VYB03975;MFCD15474877;AKOS015991440;GF-0715;SB31945;3-hydrazinobenzenesulfonamide hydrochloride;3-hydrazinylbenzenesulfonamidehydrochloride;CS-0342443;3-Hydrazino-benzenesulfonamide hydrochloride, AldrichCPR;3-Hydrazinylbenzene-1-sulfonamide--hydrogen chloride (1/1)

Chemical Property of 3-Hydrazinylbenzenesulfonamide hydrochloride

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.666
• Boiling Point: 452.611 °C at 760 mmHg
• PKA: 10.31±0.60(Predicted)
• Flash Point: 227.531 °C
• PSA: 106.59000
• Density: 1.498g/cm³
• LogP: 2.17400
• Storage Temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 223.0182254
• Heavy Atom Count: 13
• Complexity: 234

Purity/Quality:

97% ^*data from raw suppliers

3-Hydrazinylbenzene-1-sulfonamide hydrochloride >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)S(=O)(=O)N)NN.Cl

Technology Process of 3-Hydrazinylbenzenesulfonamide hydrochloride

There total 1 articles about 3-Hydrazinylbenzenesulfonamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3-hydrazino-benzenesulfonic acid amide (131774-72-6)

Guidance literature:

Diazotization_.Umsetzen mit Na₂SO₃-Loesung und Behandeln des Reaktionsprodukts mit konzentrierter Salzsaeure;

Reference yield: 37.52%

3-hydrazino-benzenesulfonic acid amide (131774-72-6) + [(fluoro-2-iodo-4)pyrid-3-yl]-carboxaldehyde (153034-82-3) → 3-(4-Iodo-1H-pyrazolo[3,4-b]pyridin-1-yl)benzenesulfonamide (1356054-64-2)

Guidance literature:

In 1-methyl-pyrrolidin-2-one; at 185 ℃; for 6.5h; Inert atmosphere; capped;

Reference yield:

3-hydrazino-benzenesulfonic acid amide (131774-72-6) + ethyl acetoacetate (141-97-9) → 1-(3-sulfoamido)-1 phenyl-3-methyl-5-pyrazolone (89-29-2)

Guidance literature:

In toluene; at 120 ℃; for 17h;

DOI:10.1002/adsc.201800464

Downstream raw materials:

3-(5-amino-3-methyl-pyrazol-1-yl)-benzenesulfonamide

6-(3-Sulfamoylphenylazo)-5-hydroxychrysen

3-(4-(4-methoxypyridin-3-yl)-1H-pyrazolo[3,4-b]pyridin-1-yl)benzenesulfonamide

1-(3-sulfamoylphenyl)-1H-pyrazolo[3,4-b]pyridin-4-ylboronic acid

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