ethyl (Z)-2-[(dimethoxyphosphoryl)methyl]-3-(4-methoxyphenyl)-2-propenoate

Base Information

Chemical Name:ethyl (Z)-2-[(dimethoxyphosphoryl)methyl]-3-(4-methoxyphenyl)-2-propenoate
CAS No.:1174757-06-2
Molecular Formula:C₁₅H₂₁O₆P
Molecular Weight:328.302
Hs Code.:

Synonyms:ethyl (Z)-2-[(dimethoxyphosphoryl)methyl]-3-(4-methoxyphenyl)-2-propenoate

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Chemical Property of ethyl (Z)-2-[(dimethoxyphosphoryl)methyl]-3-(4-methoxyphenyl)-2-propenoate

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Technology Process of ethyl (Z)-2-[(dimethoxyphosphoryl)methyl]-3-(4-methoxyphenyl)-2-propenoate

There total 5 articles about ethyl (Z)-2-[(dimethoxyphosphoryl)methyl]-3-(4-methoxyphenyl)-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 88039-45-6
ethyl 2-(hydroxy(4-methoxyphenyl)methyl)acrylate

: 3743-07-5
dimethyl chlorophosphite

: 1174757-06-2
ethyl (Z)-2-[(dimethoxyphosphoryl)methyl]-3-(4-methoxyphenyl)-2-propenoate

Guidance literature:: ethyl 2-(hydroxy(4-methoxyphenyl)methyl)acrylate; dimethyl chlorophosphite; With triethylamine; In diethyl ether; at -10 ℃; Inert atmosphere;

at 70 - 100 ℃; Inert atmosphere;
DOI:10.1021/ol9012469

Reference yield:

: C₁₅H₂₁O₆P

: 1174757-06-2
ethyl (Z)-2-[(dimethoxyphosphoryl)methyl]-3-(4-methoxyphenyl)-2-propenoate

Guidance literature:: at 70 - 100 ℃; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.12.002

Reference yield:

: 88039-45-6
ethyl 2-(hydroxy(4-methoxyphenyl)methyl)acrylate

: 1174757-06-2
ethyl (Z)-2-[(dimethoxyphosphoryl)methyl]-3-(4-methoxyphenyl)-2-propenoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / diethyl ether / 0.33 h / -10 °C / Inert atmosphere

2: 70 - 100 °C / Inert atmosphere

With triethylamine; In diethyl ether;
DOI:10.1016/j.tetasy.2011.12.002