(E)-3-(6-benzyloxy-1,2,3,5-tetramethoxy-9-oxo-9H-acridin-10-yl)acrylic acid

Base Information

Chemical Name:(E)-3-(6-benzyloxy-1,2,3,5-tetramethoxy-9-oxo-9H-acridin-10-yl)acrylic acid
CAS No.:1325207-76-8
Molecular Formula:C₂₇H₂₅NO₈
Molecular Weight:491.497
Hs Code.:

Synonyms:(E)-3-(6-benzyloxy-1,2,3,5-tetramethoxy-9-oxo-9H-acridin-10-yl)acrylic acid

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Chemical Property of (E)-3-(6-benzyloxy-1,2,3,5-tetramethoxy-9-oxo-9H-acridin-10-yl)acrylic acid

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Technology Process of (E)-3-(6-benzyloxy-1,2,3,5-tetramethoxy-9-oxo-9H-acridin-10-yl)acrylic acid

There total 6 articles about (E)-3-(6-benzyloxy-1,2,3,5-tetramethoxy-9-oxo-9H-acridin-10-yl)acrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1325207-42-8
6-benzyloxy-1,2,3,5-tetramethoxy-10H-acridin-9-one

: 623-47-2
propynoic acid ethyl ester

: 1325207-76-8
(E)-3-(6-benzyloxy-1,2,3,5-tetramethoxy-9-oxo-9H-acridin-10-yl)acrylic acid

: 1325207-46-2
(E)-3-(6-benzyloxy-1,2,3,5-tetramethoxy-9-oxo-9H-acridin-10-yl)acrylic acid

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.tet.2011.06.062

Reference yield:

: 1325207-40-6
4-benzyloxy-3-methoxy-2-(3,4,5-trimethoxyphenylamino)benzoic acid

: 1325207-76-8
(E)-3-(6-benzyloxy-1,2,3,5-tetramethoxy-9-oxo-9H-acridin-10-yl)acrylic acid

: 1325207-46-2
(E)-3-(6-benzyloxy-1,2,3,5-tetramethoxy-9-oxo-9H-acridin-10-yl)acrylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide; trichlorophosphate / 1 h / 60 °C

2: hydrogenchloride / methanol; chloroform; water / 40 °C

3: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; potassium carbonate; N,N-dimethyl-formamide; trichlorophosphate; In methanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.06.062

Reference yield:

: C₂₄H₂₄ClNO₆

: 1325207-76-8
(E)-3-(6-benzyloxy-1,2,3,5-tetramethoxy-9-oxo-9H-acridin-10-yl)acrylic acid

: 1325207-46-2
(E)-3-(6-benzyloxy-1,2,3,5-tetramethoxy-9-oxo-9H-acridin-10-yl)acrylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / methanol; chloroform; water / 40 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; potassium carbonate; In methanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.06.062