iso-propyl 7-[2-amino-2-(4-cyanophenyl)ethyl]-3,7-diazabicyclo-[3.3.1]nonane-3-carboxylate

Base Information

Chemical Name:iso-propyl 7-[2-amino-2-(4-cyanophenyl)ethyl]-3,7-diazabicyclo-[3.3.1]nonane-3-carboxylate
CAS No.:313238-19-6
Molecular Formula:C₂₀H₂₈N₄O₂
Molecular Weight:356.468
Hs Code.:

Synonyms:iso-propyl 7-[2-amino-2-(4-cyanophenyl)ethyl]-3,7-diazabicyclo-[3.3.1]nonane-3-carboxylate

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Chemical Property of iso-propyl 7-[2-amino-2-(4-cyanophenyl)ethyl]-3,7-diazabicyclo-[3.3.1]nonane-3-carboxylate

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Technology Process of iso-propyl 7-[2-amino-2-(4-cyanophenyl)ethyl]-3,7-diazabicyclo-[3.3.1]nonane-3-carboxylate

There total 1 articles about iso-propyl 7-[2-amino-2-(4-cyanophenyl)ethyl]-3,7-diazabicyclo-[3.3.1]nonane-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: iso-propyl 7-[2-azido-2-(4-cyanophenyl)ethyl]-3,7-diazabicyclo-[3.3.1]nonane-3-carboxylate

: 313238-19-6
iso-propyl 7-[2-amino-2-(4-cyanophenyl)ethyl]-3,7-diazabicyclo-[3.3.1]nonane-3-carboxylate

Guidance literature:: With hydrogen; 5%-palladium/activated carbon; In ethanol; water; under 760.051 Torr;

Reference yield: 67.0%

: 313238-19-6
iso-propyl 7-[2-amino-2-(4-cyanophenyl)ethyl]-3,7-diazabicyclo-[3.3.1]nonane-3-carboxylate

: 144-55-8
sodium hydrogencarbonate

: 1194-00-9
tetrahydro-2-isocyanato-2H-pyran

: 313238-21-0
iso-propyl 7-[2-carbamoylamino-2-(4-cyanophenyl)ethyl]-3,7-diazabicyclo[3.3.1]nonane-3-carboxylate

Guidance literature:: iso-propyl 7-[2-amino-2-(4-cyanophenyl)ethyl]-3,7-diazabicyclo-[3.3.1]nonane-3-carboxylate; tetrahydro-2-isocyanato-2H-pyran; In benzene; at 20 ℃; for 2h;

With hydrogenchloride; In methanol; water; for 3h; Heating / reflux;

sodium hydrogencarbonate; In methanol; water;

Reference yield: 45.0%

: 313238-19-6
iso-propyl 7-[2-amino-2-(4-cyanophenyl)ethyl]-3,7-diazabicyclo-[3.3.1]nonane-3-carboxylate

: 471-46-5
Oxalamide

: 313238-23-2
iso-propyl 7-[2-carbamoylcarboxamido-2-(4-cyanophenyl)ethyl]-3,7-diaza-bicyclo[3.3.1]nonane-3-carboxylate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 10h; pH=7 - 8;