Pyrrolidin-1-yl-(4-pyrrolidin-1-ylpyridin-2-yl)methanone

Base Information

• Chemical Name: Pyrrolidin-1-yl-(4-pyrrolidin-1-ylpyridin-2-yl)methanone
• CAS No.: 83728-54-5
• Molecular Formula: C₁₄H₁₉N₃O
• Molecular Weight: 245.324
• Hs Code.: 2933399990
• Mol file: 83728-54-5.mol

Synonyms:4-(pyrrolidin-1-yl)-2-pyridinecarboxylic acid pyrrolidine amide

Chemical Property of Pyrrolidin-1-yl-(4-pyrrolidin-1-ylpyridin-2-yl)methanone

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

Pyrrolidin-1-yl-(4-pyrrolidin-1-ylpyridin-2-yl)methanone 97 ^*data from reagent suppliers

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Technology Process of Pyrrolidin-1-yl-(4-pyrrolidin-1-ylpyridin-2-yl)methanone

There total 2 articles about Pyrrolidin-1-yl-(4-pyrrolidin-1-ylpyridin-2-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-Cyclopentyl-N-(4-pyrrolidin-1-yl-pyridine-2-carbonyl)-benzamide (82776-77-0) → N-cyclopentylbenzamide (53226-42-9) + 4-(pyrrolidin-1-yl)-2-pyridinecarboxylic acid pyrrolidine amide (83728-54-5)

Guidance literature:

With pyrrolidine; In acetonitrile; for 10h; Ambient temperature;

Reference yield:

pyrrolidine (123-75-1) + N-Cyclopentyl-N-(4-pyrrolidin-1-yl-pyridine-2-carbonyl)-benzamide (82776-77-0) → N-cyclopentylbenzamide (53226-42-9) + 4-(pyrrolidin-1-yl)-2-pyridinecarboxylic acid pyrrolidine amide (83728-54-5)

Guidance literature:

In acetonitrile; for 10h; Ambient temperature;

Reference yield: 91.0%

phenyllithium (591-51-5) + 4-(pyrrolidin-1-yl)-2-pyridinecarboxylic acid pyrrolidine amide (83728-54-5) → phenyl 2-(4-pyrrolidin-1-yl)pyridyl-methanone

Guidance literature:

In tetrahydrofuran; diethyl ether; cyclohexane; at -78 - 20 ℃;

DOI:10.1021/jo991202k

upstream raw materials:

pyrrolidine

N-Cyclopentyl-N-(4-pyrrolidin-1-yl-pyridine-2-carbonyl)-benzamide

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