4-fluorophenyl-O-trimethylsilylhydroxamic acid trifluoromethanesulfonylimide

Base Information

Chemical Name:4-fluorophenyl-O-trimethylsilylhydroxamic acid trifluoromethanesulfonylimide
CAS No.:1017797-17-9
Molecular Formula:C₁₁H₁₄F₄N₂O₃SSi
Molecular Weight:358.389
Hs Code.:

Synonyms:4-fluorophenyl-O-trimethylsilylhydroxamic acid trifluoromethanesulfonylimide

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Chemical Property of 4-fluorophenyl-O-trimethylsilylhydroxamic acid trifluoromethanesulfonylimide

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Technology Process of 4-fluorophenyl-O-trimethylsilylhydroxamic acid trifluoromethanesulfonylimide

There total 2 articles about 4-fluorophenyl-O-trimethylsilylhydroxamic acid trifluoromethanesulfonylimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1017797-05-5
4-fluorophenylhydroxamic acid trifluoromethanesulfonylimide

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 1017797-17-9
4-fluorophenyl-O-trimethylsilylhydroxamic acid trifluoromethanesulfonylimide

Guidance literature:: In acetonitrile; at 20 ℃; for 72h;
DOI:10.1016/j.jfluchem.2007.01.002

Reference yield:

: 42202-95-9
4-fluoro-N-hydroxybenzimidoyl chloride

: 1017797-17-9
4-fluorophenyl-O-trimethylsilylhydroxamic acid trifluoromethanesulfonylimide

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / dimethylformamide / 24 h / 20 °C

2: 91 percent / acetonitrile / 72 h / 20 °C

In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.jfluchem.2007.01.002

Reference yield: 6.0%

: 110-91-8,99108-56-2
morpholine

: 1017797-17-9
4-fluorophenyl-O-trimethylsilylhydroxamic acid trifluoromethanesulfonylimide

: N-(4-fluorophenyl)-N'-trifluoromethylsulfonylurea

: 4-[N-(4-fluorophenyl)-N'-trifluoromethylsulfonylamidino]morpholine

Guidance literature:: 4-fluorophenyl-O-trimethylsilylhydroxamic acid trifluoromethanesulfonylimide; In toluene; for 0.5h; Heating;

morpholine; In 1,2-dimethoxyethane; at 20 ℃; for 24h; Further stages.;
DOI:10.1016/j.jfluchem.2007.01.002