4-fluorophenylhydroxamic acid trifluoromethanesulfonylimide

Base Information

• Chemical Name: 4-fluorophenylhydroxamic acid trifluoromethanesulfonylimide
• CAS No.: 1017797-05-5
• Molecular Formula: C₈H₆F₄N₂O₃S
• Molecular Weight: 286.207

Synonyms:4-fluorophenylhydroxamic acid trifluoromethanesulfonylimide

Chemical Property of 4-fluorophenylhydroxamic acid trifluoromethanesulfonylimide

Chemical Property:

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Technology Process of 4-fluorophenylhydroxamic acid trifluoromethanesulfonylimide

There total 1 articles about 4-fluorophenylhydroxamic acid trifluoromethanesulfonylimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

4-fluoro-N-hydroxybenzimidoyl chloride (42202-95-9) + trifluoromethanesulphonamide sodium salt (35534-15-7) → 4-fluorophenylhydroxamic acid trifluoromethanesulfonylimide (1017797-05-5)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1016/j.jfluchem.2007.01.002

Reference yield: 91.0%

4-fluorophenylhydroxamic acid trifluoromethanesulfonylimide (1017797-05-5) + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) → 4-fluorophenyl-O-trimethylsilylhydroxamic acid trifluoromethanesulfonylimide (1017797-17-9)

Guidance literature:

In acetonitrile; at 20 ℃; for 72h;

DOI:10.1016/j.jfluchem.2007.01.002

Reference yield: 85.0%

4-fluorophenylhydroxamic acid trifluoromethanesulfonylimide (1017797-05-5) → N-trifluoromethylsulfonyl-N'-4-fluorophenylchloroformamidine

Guidance literature:

With thionyl chloride; In 1,2-dimethoxyethane; for 1h; Heating;

DOI:10.1016/j.jfluchem.2007.01.002

upstream raw materials:

4-fluoro-N-hydroxybenzimidoyl chloride

trifluoromethanesulphonamide sodium salt

Downstream raw materials:

4-fluorophenyl-O-trimethylsilylhydroxamic acid trifluoromethanesulfonylimide

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