5,5′-bis(dimesitylboranyl)-2,2′-bipyridine

Base Information

Chemical Name:5,5′-bis(dimesitylboranyl)-2,2′-bipyridine
CAS No.:944393-86-6
Molecular Formula:C₄₆H₅₀B₂N₂
Molecular Weight:652.538
Hs Code.:

Synonyms:5,5′-bis(dimesitylboranyl)-2,2′-bipyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,5′-bis(dimesitylboranyl)-2,2′-bipyridine

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Technology Process of 5,5′-bis(dimesitylboranyl)-2,2′-bipyridine

There total 2 articles about 5,5′-bis(dimesitylboranyl)-2,2′-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 15862-18-7
5,5'-dibromo-2,2'-dipyridyl

: 436-59-9
dimesitylfluoroborane

: 944393-86-6
5,5′-bis(dimesitylboranyl)-2,2′-bipyridine

Guidance literature:: 5,5'-dibromo-2,2'-dipyridyl; With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane; at -100 ℃; for 1h;

dimesitylfluoroborane; In tetrahydrofuran; diethyl ether; hexane; at -100 - 20 ℃; Further stages.;
DOI:10.1021/ja0725652

Reference yield: 58.0%

: 5,5'-(Li)2-2,2'-bipy

: 436-59-9
dimesitylfluoroborane

: 944393-86-6
5,5′-bis(dimesitylboranyl)-2,2′-bipyridine

Guidance literature:: In not given; react. BMes2F and 5,5'-(Li)2-2,2'-bipy (2.1:1) at -100°C;
DOI:10.1021/ja0725652

Reference yield: 84.0%

: 944393-86-6
5,5′-bis(dimesitylboranyl)-2,2′-bipyridine

: 10025-99-7
potassium tetrachloroplatinate(II)

: 1137719-52-8
Pt(5,5'-bis(B(mesityl)2)-2,2'-bipyridine)Cl₂

Guidance literature:: In dichloromethane; water; dimethyl sulfoxide; under N2; ligand in CH2Cl2 added to stirred soln. of K2PtCl4 in H2O-DMSO; stirred at room temp. for 6 h; org. phase sepd.; pptd. by hexane; washed with Et2O; elem. anal.;
DOI:10.1021/ic9000335