3-[2-(3-Bromo-5-nitro-phenyl)-2-chloro-ethyl]-thiazolidin-2-ylideneamine

Base Information

Chemical Name:3-[2-(3-Bromo-5-nitro-phenyl)-2-chloro-ethyl]-thiazolidin-2-ylideneamine
CAS No.:145028-82-6
Molecular Formula:C₁₁H₁₁BrClN₃O₂S
Molecular Weight:364.65
Hs Code.:

Synonyms:3-[2-(3-Bromo-5-nitro-phenyl)-2-chloro-ethyl]-thiazolidin-2-ylideneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-[2-(3-Bromo-5-nitro-phenyl)-2-chloro-ethyl]-thiazolidin-2-ylideneamine

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Technology Process of 3-[2-(3-Bromo-5-nitro-phenyl)-2-chloro-ethyl]-thiazolidin-2-ylideneamine

There total 2 articles about 3-[2-(3-Bromo-5-nitro-phenyl)-2-chloro-ethyl]-thiazolidin-2-ylideneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6307-83-1
3-bromo-5-nitro-benzoic acid

: 145028-82-6
3-[2-(3-Bromo-5-nitro-phenyl)-2-chloro-ethyl]-thiazolidin-2-ylideneamine

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / dimethylformamide / 3 h / Heating

2: 2.) 48percent HBr / 1.) CHCl₃, ether, from -50 deg C to RT, 2.) CH₂Cl₂, RT, 1 h

3: acetone / 1.) RT, 1 h, 2.) reflux, 0.5 h

4: NaBH₄ / methanol / 1 h / Ambient temperature

5: SOCl₂ / CHCl₃ / 1 h / Heating

With sodium tetrahydroborate; thionyl chloride; hydrogen bromide; In methanol; chloroform; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0223-5234(92)90184-3