C₇₂H₁₁₁NO₁₃S

Base Information

Chemical Name:C₇₂H₁₁₁NO₁₃S
CAS No.:1234307-13-1
Molecular Formula:C₇₂H₁₁₁NO₁₃S
Molecular Weight:1230.74
Hs Code.:

C<sub>72</sub>H<sub>111</sub>NO<sub>13</sub>S

Synonyms:C₇₂H₁₁₁NO₁₃S

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Chemical Property of C₇₂H₁₁₁NO₁₃S

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Technology Process of C₇₂H₁₁₁NO₁₃S

There total 8 articles about C₇₂H₁₁₁NO₁₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.8%

: 1234307-02-8
C₃₆H₄₃NO₁₁S

: 112-76-5
Stearoyl chloride

: 1234307-13-1
C₇₂H₁₁₁NO₁₃S

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 2280-44-6
D-Glucose

: 1234307-13-1
C₇₂H₁₁₁NO₁₃S

Guidance literature:: Multi-step reaction with 8 steps

1.1: trifluorormethanesulfonic acid / 48 h / 0 - 80 °C

1.2: 4 h / 40 °C

2.1: sodium hydroxide / N,N-dimethyl-formamide / 24 h / 20 °C

3.1: water; acetic acid / 1 h / Reflux

4.1: dmap; pyridine / 16 h / 0 °C

5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; pyridine / dichloromethane / 18 h / 20 °C

6.1: N,N-dimethyl-formamide / 3 h / 90 °C

7.1: trimethylamine-N-oxide; water / osmium(VIII) oxide / tert-butyl alcohol / 24 h / 20 °C

8.1: pyridine / dichloromethane / 2 h / 20 °C

With pyridine; dmap; trimethylamine-N-oxide; trifluorormethanesulfonic acid; water; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; osmium(VIII) oxide; In dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 103833-57-4
allyl 4,6-O-benzylidene-2,3-di-O-benzyl-α-D-glucopyranoside

: 1234307-13-1
C₇₂H₁₁₁NO₁₃S

Guidance literature:: Multi-step reaction with 6 steps

1: water; acetic acid / 1 h / Reflux

2: dmap; pyridine / 16 h / 0 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; pyridine / dichloromethane / 18 h / 20 °C

4: N,N-dimethyl-formamide / 3 h / 90 °C

5: trimethylamine-N-oxide; water / osmium(VIII) oxide / tert-butyl alcohol / 24 h / 20 °C

6: pyridine / dichloromethane / 2 h / 20 °C

With pyridine; dmap; trimethylamine-N-oxide; water; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; osmium(VIII) oxide; In dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;