3-(3-chloropropyl)-3-(hydroxymethyl)-2-(trimethylstannyl)-2-cyclohexene

Base Information

Chemical Name:3-(3-chloropropyl)-3-(hydroxymethyl)-2-(trimethylstannyl)-2-cyclohexene
CAS No.:152564-14-2
Molecular Formula:C₁₃H₂₅ClOSn
Molecular Weight:351.504
Hs Code.:

Synonyms:3-(3-chloropropyl)-3-(hydroxymethyl)-2-(trimethylstannyl)-2-cyclohexene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3-chloropropyl)-3-(hydroxymethyl)-2-(trimethylstannyl)-2-cyclohexene

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Technology Process of 3-(3-chloropropyl)-3-(hydroxymethyl)-2-(trimethylstannyl)-2-cyclohexene

There total 1 articles about 3-(3-chloropropyl)-3-(hydroxymethyl)-2-(trimethylstannyl)-2-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 93512-05-1
methyl 1-(3-chloropropyl)-2-(trimethylstannyl)-2-cyclohexenecarboxylate

: 1191-15-7
diisobutylaluminium hydride

: 152564-14-2
3-(3-chloropropyl)-3-(hydroxymethyl)-2-(trimethylstannyl)-2-cyclohexene

Guidance literature:: With ammonium chloride; In diethyl ether; hexane; Ar; addn. of a solution of i-Bu2AlH in hexanes to a solution of the starting compound in ether at -20 ° C; stirring at -20 ° C for 1 h;; addn. of aqueous NH4Cl, stirring at rrom temperature until the organic phase was clear; filtration (florisil, ether); concentration; distillation (125-130 ° C/0.1 Torr);;