[chloro(bis[(2-diphenylphosphino)ethyl]amine)palladium(II)] chloride monohydrate

Base Information

Chemical Name:[chloro(bis[(2-diphenylphosphino)ethyl]amine)palladium(II)] chloride monohydrate
CAS No.:233748-27-1
Molecular Formula:C₂₈H₂₉ClNP₂Pd*Cl*H₂O
Molecular Weight:636.834
Hs Code.:

Synonyms:[chloro(bis[(2-diphenylphosphino)ethyl]amine)palladium(II)] chloride monohydrate

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Chemical Property of [chloro(bis[(2-diphenylphosphino)ethyl]amine)palladium(II)] chloride monohydrate

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Technology Process of [chloro(bis[(2-diphenylphosphino)ethyl]amine)palladium(II)] chloride monohydrate

There total 2 articles about [chloro(bis[(2-diphenylphosphino)ethyl]amine)palladium(II)] chloride monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 7732-18-5
water

: 66534-97-2
bis(2-(diphenylphosphino)ethyl)amine hydrochloride

: palladium dichloride

: 233748-27-1
[chloro(bis[(2-diphenylphosphino)ethyl]amine)palladium(II)] chloride monohydrate

Guidance literature:: With NaCl; In dichloromethane; water; suspn. of Pd and Na compds. in water heated at 80°C, after dissolving cooled to room temp., soln. of org. compd. in CH2Cl2 added dropwise, stirred for 15 h at room temp.; org. phase extd. with CH2Cl2, dried with Na2SO4, filtered, solvent removed in vac., recrystd. from CH2Cl2-n-hexane, elem. anal.;
DOI:10.1039/b109675n

Reference yield: 90.0%

: 10025-98-6
potassium tetrachloropalladate(II)

: 66534-96-1
bis[(2-diphenylphosphino)ethyl]amine hydrochloride

: 7732-18-5
water

: 233748-27-1
[chloro(bis[(2-diphenylphosphino)ethyl]amine)palladium(II)] chloride monohydrate

Guidance literature:: In dichloromethane; water; a soln. of P compd. (CH2Cl2) added dropwise to a soln. of Pd compd. (H2O, 1 equiv.), stirred for 1-24 h at room temp.; concd. (vac.), diethyl ether added, ppt. filtered, washed (H2O), dried vac.), recrystd. (CH2Cl2/hexane), dried (vac.); elem. anal.;
DOI:10.1016/j.ica.2005.03.018

Reference yield: 87.0%

: 67-56-1
methanol

: 233748-27-1
[chloro(bis[(2-diphenylphosphino)ethyl]amine)palladium(II)] chloride monohydrate

: silver nitrate

: [Pd(bis[2-(diphenylphosphino)ethyl]amine)ONO₂]NO₃*CH₃OH

Guidance literature:: In methanol; chloroform; byproducts: AgCl; soln. of AgNO3 in MeOH added dropwise to soln. of Pd compd. in CHCl3, kept for 20 h in dark; filtered, solvent removed in vac., recrystd. from CH2Cl2-n-hexane, elem.anal.;
DOI:10.1039/b109675n