Technology Process of C23H36N2O3Si
There total 5 articles about C23H36N2O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C16H32O4Si; N,N-dimethyl-formamide dimethyl acetal;
at 80 ℃;
for 4h;
phenylhydrazine;
In
ethanol;
at 80 ℃;
for 6h;
DOI:10.1016/j.bmcl.2013.01.090
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C
1.2: 20 °C
2.1: hydrogen; palladium on activated charcoal / 20 °C
2.2: 20 °C
3.1: tert-butyl alcohol; sodium chlorite; sodium dihydrogenphosphate / water / 20 °C
4.1: 1,1'-carbonyldiimidazole; triethylamine / acetonitrile / 2 h / 90 °C
5.1: 4 h / 80 °C
5.2: 6 h / 80 °C
With
sodium chlorite; sodium dihydrogenphosphate; lithium aluminium tetrahydride; palladium on activated charcoal; hydrogen; triethylamine; 1,1'-carbonyldiimidazole; tert-butyl alcohol;
In
tetrahydrofuran; water; acetonitrile;
DOI:10.1016/j.bmcl.2013.01.090
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogen; palladium on activated charcoal / 20 °C
1.2: 20 °C
2.1: tert-butyl alcohol; sodium chlorite; sodium dihydrogenphosphate / water / 20 °C
3.1: 1,1'-carbonyldiimidazole; triethylamine / acetonitrile / 2 h / 90 °C
4.1: 4 h / 80 °C
4.2: 6 h / 80 °C
With
sodium chlorite; sodium dihydrogenphosphate; palladium on activated charcoal; hydrogen; triethylamine; 1,1'-carbonyldiimidazole; tert-butyl alcohol;
In
water; acetonitrile;
DOI:10.1016/j.bmcl.2013.01.090
