2-ACETYL-4'-CHLORO DIPHENYL SULFIDE

Base Information

• Chemical Name: 2-ACETYL-4'-CHLORO DIPHENYL SULFIDE
• CAS No.: 41932-35-8
• Molecular Formula: C14H11 Cl O S
• Molecular Weight: 262.76
• Hs Code.: 2930909090
• Mol file: 41932-35-8.mol

Synonyms:1-[2-[(4-Chlorophenyl)thio]phenyl]ethanone

Chemical Property of 2-ACETYL-4'-CHLORO DIPHENYL SULFIDE

Chemical Property:

• Vapor Pressure: 7.5E-06mmHg at 25°C
• Boiling Point: 376°C at 760 mmHg
• Flash Point: 181.2°C
• PSA: 42.37000
• Density: 1.28g/cm³
• LogP: 4.69380

Purity/Quality:

98% or more ^*data from raw suppliers

2-Acetyl-4'-chloro diphenylsulfide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-ACETYL-4'-CHLORO DIPHENYL SULFIDE

There total 4 articles about 2-ACETYL-4'-CHLORO DIPHENYL SULFIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

para-chlorothiophenol + 2-nitroacetophenone (614-21-1) → 1-[2-(4-chloro-phenylsulfanyl)-phenyl]-ethanone (41932-35-8)

Guidance literature:

With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 50 ℃; for 16h;

Reference yield:

p-Chlorothiophenol (106-54-7) + 2-nitroacetophenone (614-21-1) → 1-[2-(4-chloro-phenylsulfanyl)-phenyl]-ethanone (41932-35-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide;

Reference yield:

2-<4-Chlor-phenylthio>-benzoesaeurechlorid (6469-86-9) + diethyl malonate (105-53-3) → 1-[2-(4-chloro-phenylsulfanyl)-phenyl]-ethanone (41932-35-8)

Guidance literature:

Multistep reaction; (i) Mg, EtOH, CCl₄, Et₂O, (ii) /BRN= 2696447/, (iii) aq. H₂SO₄, AcOH;

upstream raw materials:

2-<4-Chlor-phenylthio>-benzoesaeurechlorid

diethyl malonate

2-nitroacetophenone

p-Chlorothiophenol

Downstream raw materials:

ethyl 3-{2-[(4-chlorophenyl)thio]phenyl}-2-butenoate

2-carboxyphenyl 4-chlorophenyl sulphide

(2-(4-chlorophenylthio)phenyl)methanol

2-[2-(4-chlorophenyl)sulfanylphenyl]acetic acid

Refernces

• 1、 -. "Novel amides that activate soluble guanylate cyclase". . . Retrieved 2008/06/13.