Ru(CO)(1-(2-aminophenyl)-2,2-dimethyl-1-propanone(-1H))(PPh₃)(t-BuC(O)C₆H₄)

Base Information

• Chemical Name: Ru(CO)(1-(2-aminophenyl)-2,2-dimethyl-1-propanone(-1H))(PPh₃)(t-BuC(O)C₆H₄)
• CAS No.: 1147856-76-5
• Molecular Formula: C₄₁H₄₃NO₃PRu
• Molecular Weight: 729.841

Synonyms:Ru(CO)(1-(2-aminophenyl)-2,2-dimethyl-1-propanone(-1H))(PPh₃)(t-BuC(O)C₆H₄)

Chemical Property of Ru(CO)(1-(2-aminophenyl)-2,2-dimethyl-1-propanone(-1H))(PPh₃)(t-BuC(O)C₆H₄)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ru(CO)(1-(2-aminophenyl)-2,2-dimethyl-1-propanone(-1H))(PPh₃)(t-BuC(O)C₆H₄)

There total 7 articles about Ru(CO)(1-(2-aminophenyl)-2,2-dimethyl-1-propanone(-1H))(PPh₃)(t-BuC(O)C₆H₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II) (25360-32-1,22337-78-6) + 1-(2-aminophenyl)-2,2-dimethylpropan-1-one (65374-14-3) → Ru(CO)(1-(2-aminophenyl)-2,2-dimethyl-1-propanone(-1H))(PPh3)(t-BuC(O)C6H4) (1147856-76-5) + ammonia (7664-41-7)

Guidance literature:

With tert-butylethylene; In toluene; at 120 ℃; for 20h; Reagent/catalyst; Inert atmosphere;

DOI:10.1021/om3011855

Reference yield: 6.0%

carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II) (25360-32-1,22337-78-6) + 1-(2-aminophenyl)-2,2-dimethylpropan-1-one (65374-14-3) → Ru(CO)(1-(2-aminophenyl)-2,2-dimethyl-1-propanone(-1H))(PPh3)(t-BuC(O)C6H4) (1147856-76-5) + RuH(CO)(1-(2-aminophenyl)-2,2-dimethyl-1-propanone(-1H))(PPh3)2 (1147856-75-4)

Guidance literature:

In toluene; at 120 ℃; for 72h; Inert atmosphere;

DOI:10.1021/om3011855

Reference yield:

carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II) (25360-32-1,22337-78-6) + 1-(2-aminophenyl)-2,2-dimethylpropan-1-one (65374-14-3) → Ru(CO)(1-(2-aminophenyl)-2,2-dimethyl-1-propanone(-1H))(PPh3)(t-BuC(O)C6H4) (1147856-76-5)

Guidance literature:

With ethenyltrimethylsilane; In ⁽²⁾H₈-toluene; at 120 ℃; for 20h; Reagent/catalyst; Time; Inert atmosphere; Glovebox;

DOI:10.1021/om3011855

upstream raw materials:

Ru(CO)(PPh₃)₃

carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II)

1-(2-aminophenyl)-2,2-dimethylpropan-1-one

RuH(CO)(1-(2-aminophenyl)-2,2-dimethyl-1-propanone(-1H))(PPh₃)₂

Downstream raw materials:

Ru(CO)(1-(2-amino-5-methylphenyl)-2,2-dimethyl-1-propanone(-1H))(PPh₃)(t-BuC(O)C₆H₄)

Ru(CO)(1-(6-amino-3-methoxyphenyl)-2,2-dimethyl-1-propanone(-1H))(PPh₃)(t-BuC(O)C₆H₄)

Ru(CO)(1-(6-amino-3-fluorophenyl)-2,2-dimethyl-1-propanone(-1H))(PPh₃)(t-BuC(O)C₆H₄)

Ru(CO)(1-{2-amino-5-(trifluoromethyl)phenyl}-2,2-dimethyl-1-propanone(-1H))(PPh₃)(t-BuC(O)C₆H₄)

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