Technology Process of C59H45NO2
There total 5 articles about C59H45NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2,6-bis<4-bromophenyl>pyridine; 2-[1-(4-methoxyphenyl)-2,2-diphenylvinyl]-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane;
With
Aliquat 336; potassium carbonate;
In
water; toluene;
Inert atmosphere;
With
tetrakis(triphenylphosphine) palladium(0);
In
water; toluene;
at 90 ℃;
for 16h;
Inert atmosphere;
DOI:10.1016/j.tet.2012.06.096
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: bis-triphenylphosphine-palladium(II) chloride; potassium phenolate; triphenylphosphine / toluene / 12 h / 70 °C / Inert atmosphere
2.1: Aliquat 336; potassium carbonate / water; toluene / Inert atmosphere
2.2: 16 h / 90 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; potassium phenolate; Aliquat 336; potassium carbonate; triphenylphosphine;
In
water; toluene;
2.1: Suzuki cross-coupling / 2.2: Suzuki cross-coupling;
DOI:10.1016/j.tet.2012.06.096
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: bromine / chloroform / 20 °C / Inert atmosphere
2.1: bis-triphenylphosphine-palladium(II) chloride; potassium phenolate; triphenylphosphine / toluene / 12 h / 70 °C / Inert atmosphere
3.1: Aliquat 336; potassium carbonate / water; toluene / Inert atmosphere
3.2: 16 h / 90 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; potassium phenolate; bromine; Aliquat 336; potassium carbonate; triphenylphosphine;
In
chloroform; water; toluene;
3.1: Suzuki cross-coupling / 3.2: Suzuki cross-coupling;
DOI:10.1016/j.tet.2012.06.096
