C₂₇H₂₂F₁₇NO₄S

Base Information

• Chemical Name: C₂₇H₂₂F₁₇NO₄S
• CAS No.: 1307800-58-3
• Molecular Formula: C₂₇H₂₂F₁₇NO₄S
• Molecular Weight: 779.515
• Mol file: 1307800-58-3.mol

Synonyms:C₂₇H₂₂F₁₇NO₄S

Chemical Property of C₂₇H₂₂F₁₇NO₄S

Chemical Property:

Purity/Quality:

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Technology Process of C₂₇H₂₂F₁₇NO₄S

There total 1 articles about C₂₇H₂₂F₁₇NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

ethanol (64-17-5) + C15H5F17O4S (731857-74-2) + isobutyraldehyde (78-84-2) + aniline (62-53-3) → C27H22F17NO4S (1307800-58-3)

Guidance literature:

With ytterbium(III) triflate; In ethanol; at 50 ℃; for 0.333333h; Microwave irradiation;

DOI:10.1039/c0gc00725k

Reference yield: 68.0%

4-hydroxy[1]benzopyran-2-one (1076-38-6,92395-12-5) + C27H22F17NO4S (1307800-58-3) → C34H20F17NO6S (1307800-64-1)

Guidance literature:

With toluene-4-sulfonic acid; In 1,2-dichloro-ethane; at 85 ℃; for 0.5h; Microwave irradiation;

DOI:10.1039/c0gc00725k

Reference yield: 55.0%

4-hydroxy-1-methyl-2(1H)-quinolone (1677-46-9) + C27H22F17NO4S (1307800-58-3) → C35H23F17N2O5S (1307800-61-8)

Guidance literature:

With toluene-4-sulfonic acid; In 1,2-dichloro-ethane; at 85 ℃; for 0.5h; Microwave irradiation;

DOI:10.1039/c0gc00725k

upstream raw materials:

ethanol

C₁₅H₅F₁₇O₄S

isobutyraldehyde

aniline

Downstream raw materials:

C₃₄H₂₀F₁₇NO₆S

C₃₅H₂₃F₁₇N₂O₅S