4-methyl-N-[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]-3-nitrobenzamide hydrochloride

Base Information

Chemical Name:4-methyl-N-[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]-3-nitrobenzamide hydrochloride
CAS No.:1449570-25-5
Molecular Formula:C₁₉H₁₅F₃N₄O₃*ClH
Molecular Weight:440.809
Hs Code.:

Synonyms:4-methyl-N-[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]-3-nitrobenzamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-N-[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]-3-nitrobenzamide hydrochloride

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Technology Process of 4-methyl-N-[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]-3-nitrobenzamide hydrochloride

There total 4 articles about 4-methyl-N-[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]-3-nitrobenzamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 641571-11-1
3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)aniline

: 10397-30-5
4-methyl-3-nitrobenzoyl chloride

: 1449570-25-5
4-methyl-N-[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]-3-nitrobenzamide hydrochloride

Guidance literature:: In chloroform; N,N-dimethyl-formamide; at 10 - 20 ℃; for 5h;
DOI:10.14233/ajchem.2013.14247

Reference yield:

: 3-amino-4-methylbenzoyl chloride

: 641571-11-1
3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)aniline

: 1449570-25-5
4-methyl-N-[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]-3-nitrobenzamide hydrochloride

Guidance literature:: In chloroform; at 10 - 20 ℃;

Reference yield:

: 96-98-0
4-methyl-3-nitrobenzoic acid

: 1449570-25-5
4-methyl-N-[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]-3-nitrobenzamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / chloroform; N,N-dimethyl-formamide / 3 h / Reflux

2: chloroform; N,N-dimethyl-formamide / 5 h / 10 - 20 °C

With thionyl chloride; In chloroform; N,N-dimethyl-formamide;
DOI:10.14233/ajchem.2013.14247