N-((1R,3R,4S,6S)-4-hydroxy-4,7,7-trimethylbicyclo[4.1.0]heptan-3-yl)-4-methylbenzenesulfonamide

Base Information

• Chemical Name: N-((1R,3R,4S,6S)-4-hydroxy-4,7,7-trimethylbicyclo[4.1.0]heptan-3-yl)-4-methylbenzenesulfonamide
• CAS No.: 1187848-46-9
• Molecular Formula: C₁₇H₂₅NO₃S
• Molecular Weight: 323.456

Synonyms:N-((1R,3R,4S,6S)-4-hydroxy-4,7,7-trimethylbicyclo[4.1.0]heptan-3-yl)-4-methylbenzenesulfonamide

Chemical Property of N-((1R,3R,4S,6S)-4-hydroxy-4,7,7-trimethylbicyclo[4.1.0]heptan-3-yl)-4-methylbenzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-((1R,3R,4S,6S)-4-hydroxy-4,7,7-trimethylbicyclo[4.1.0]heptan-3-yl)-4-methylbenzenesulfonamide

There total 1 articles about N-((1R,3R,4S,6S)-4-hydroxy-4,7,7-trimethylbicyclo[4.1.0]heptan-3-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

(+)-Δ3-carene (498-15-7,19079-29-9) + chloroamine-T (127-65-1) → N-((1R,3R,4S,6S)-4-hydroxy-4,7,7-trimethylbicyclo[4.1.0]heptan-3-yl)-4-methylbenzenesulfonamide (1187848-46-9)

Guidance literature:

(+)-Δ³-carene; chloroamine-T; With osmium(VIII) oxide; water; In tert-butyl alcohol; for 18h; Reflux;

With sodium tetrahydroborate; In water; tert-butyl alcohol; at 20 ℃; for 1h; stereoselective reaction;

DOI:10.1016/j.tetasy.2009.06.007

Reference yield: 89.0%

N-((1R,3R,4S,6S)-4-hydroxy-4,7,7-trimethylbicyclo[4.1.0]heptan-3-yl)-4-methylbenzenesulfonamide (1187848-46-9) + methyl iodide (74-88-4) → N-((1R,3R,4S,6S)-4-hydroxy-4,7,7-trimethylbicyclo[4.1.0]heptan-3-yl)-N-4-dimethylbenzenesulfonamide (1187848-47-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

DOI:10.1016/j.tetasy.2009.06.007

upstream raw materials:

(+)-Δ³-carene

chloroamine-T

Downstream raw materials:

N-((1R,3R,4S,6S)-4-hydroxy-4,7,7-trimethylbicyclo[4.1.0]heptan-3-yl)-N-4-dimethylbenzenesulfonamide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1187848-46-9 N-((1R,3R,4S,6S)-4-hydroxy-4,7,7-trimethylbicyclo[4.1.0]heptan-3-yl)-4-methylbenzenesulfonamide

Send

Send

Metric Ton KG G Pound L ML

Send

Send