[Ru(II)(2,2'-bipyridine)2(6-p-anisyl-2-(p-anisylamino)-3(4H)-p-anisylimine-9-methoxyphenazine(-H))]ClO₄

Base Information

• Chemical Name: [Ru(II)(2,2'-bipyridine)2(6-p-anisyl-2-(p-anisylamino)-3(4H)-p-anisylimine-9-methoxyphenazine(-H))]ClO₄
• CAS No.: 957110-69-9
• Molecular Formula: C₅₄H₄₅N₈O₄Ru*ClO₄
• Molecular Weight: 1070.52

Synonyms:[Ru(II)(2,2'-bipyridine)2(6-p-anisyl-2-(p-anisylamino)-3(4H)-p-anisylimine-9-methoxyphenazine(-H))]ClO₄

Chemical Property of [Ru(II)(2,2'-bipyridine)2(6-p-anisyl-2-(p-anisylamino)-3(4H)-p-anisylimine-9-methoxyphenazine(-H))]ClO₄

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Technology Process of [Ru(II)(2,2'-bipyridine)2(6-p-anisyl-2-(p-anisylamino)-3(4H)-p-anisylimine-9-methoxyphenazine(-H))]ClO₄

There total 1 articles about [Ru(II)(2,2'-bipyridine)2(6-p-anisyl-2-(p-anisylamino)-3(4H)-p-anisylimine-9-methoxyphenazine(-H))]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

methanol (67-56-1) + cis-bis-(2,2′-bipyridine) dichlororuthenium(II) dihydrate + 7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine (306970-26-3) + perchlorate(1-) (14797-73-0,1059018-91-5) → [Ru(II)(2,2'-bipyridine)2(6-p-anisyl-2-(p-anisylamino)-3(4H)-p-anisylimine-9-methoxyphenazine(-H))]ClO4 (957110-69-9) + [Ru(II)(2,2'-bipyridine)2(7-methoxy-5-(4-methoxyphenylimino)-3,5-dihydro-2H-phenazin-1-one))][ClO4]2 + [Ru2(2,2'-bipyridine)4(7,8'-dimethoxy-5,10'-bis(4-methoxyphenyl)-2,3'-bis(4-methoxyphenylamino)-3,2'-bis(4-methoxyphenylimine)-..

Guidance literature:

With AgNO₃; triethyl amine; air; In methanol; byproducts: AgCl; mixt. of Ru(bpy)2Cl2*2H2O (0.125 mmol) and AgNO3 (0.25 mmol) in MeOH refluxed for 2 h, filtered, phenazine deriv. (0.125 mmol) and two drops of Et3N added to filtrate, mixt. refluxed for 6 h; concd., poured into Et2O, ppt. sepd., mixt. sepd. by repeated preparative TLC (Al2O3, CHCl3 and CHCl3/CH3CN), recrystn. (CH2Cl2/hexane); elem. anal.;

DOI:10.1002/ejic.200600864

Reference yield: 90.0%

[Ru(II)(2,2'-bipyridine)2(6-p-anisyl-2-(p-anisylamino)-3(4H)-p-anisylimine-9-methoxyphenazine(-H))]ClO4 (957110-69-9) → [Ru(II)(2,2'-bipyridine)2(7-methoxy-5-(4-methoxyphenylimino)-3,5-dihydro-2H-phenazin-1-one))][ClO4]2

Guidance literature:

With air; In methanol; water; soln. of Ru compd. in water/methanol (1:9) refluxed for 0.5 h; evapd., chromd. (Al2O3, CHCl3/CH3CN (3/2)), recrystd. (CH3CN/toluene);

DOI:10.1002/ejic.200600864

Reference yield: 75.0%

[Ru(II)(2,2'-bipyridine)2(6-p-anisyl-2-(p-anisylamino)-3(4H)-p-anisylimine-9-methoxyphenazine(-H))]ClO4 (957110-69-9) → [Ru(II)(2,2'-bipyridine)2(7-methoxy-5-(4-methoxyphenylimino)-3,5-dihydro-2H-phenazin-1-one))][ClO4]2 + [Ru2(2,2'-bipyridine)4(7,8'-dimethoxy-5,10'-bis(4-methoxyphenyl)-2,3'-bis(4-methoxyphenylamino)-3,2'-bis(4-methoxyphenylimine)-..

Guidance literature:

In methanol; soln. of Ru compd. in MeOH refluxed under N2 for 6 h; evapd. to dryness, TLC (Al2O3, CHCl3/CH3CN 3/2), recrystd. (CH3CN/toluene);

DOI:10.1002/ejic.200600864

upstream raw materials:

methanol

7-methoxy-N,5-bis(4-methoxyphenyl)-3-(4-methoxyphenylimino)-3,5-dihydrophenazin-2-amine

perchlorate^(1-)

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