(3,5-cycloheptadienyl)diphenylphosphine

Base Information

Chemical Name:(3,5-cycloheptadienyl)diphenylphosphine
CAS No.:1355338-85-0
Molecular Formula:C₁₉H₁₉P
Molecular Weight:278.334
Hs Code.:

Synonyms:(3,5-cycloheptadienyl)diphenylphosphine

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Chemical Property of (3,5-cycloheptadienyl)diphenylphosphine

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Technology Process of (3,5-cycloheptadienyl)diphenylphosphine

There total 1 articles about (3,5-cycloheptadienyl)diphenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 544-25-2
Cyclohepta-1,3,5-triene

: 829-85-6
diphenylphosphane

: 1355338-85-0
(3,5-cycloheptadienyl)diphenylphosphine

Guidance literature:: diphenylphosphane; With n-butyllithium; In hexane; toluene; at 20 ℃; for 0.5h; Inert atmosphere;

Cyclohepta-1,3,5-triene; In hexane; toluene; at 70 ℃; for 18h; Inert atmosphere;
DOI:10.1021/om200999n

Reference yield: 98.0%

: 1355338-85-0
(3,5-cycloheptadienyl)diphenylphosphine

: palladium dichloride

: 1355338-87-2
cis-dichlorobis((3,5-cycloheptadienyl)diphenylphosphine)palladium(II)

Guidance literature:: In dichloromethane; under Ar; ligand dissolved in CH2Cl2; added over 5 min to soln. of PdCl2in CH2Cl2; stirred at room temp. for 18 h; soln. filtered over Celite; evapd. under reduced pressure; triturated with pentane; solid rinsed with pentane;
DOI:10.1021/om200999n

Reference yield: 97.0%

: 12080-32-9
dichloro( 1,5-cyclooctadiene)platinum(ll)

: 1355338-85-0
(3,5-cycloheptadienyl)diphenylphosphine

: 1355338-86-1
cis-dichlorobis((3,5-cycloheptadienyl)diphenylphosphine)platinum(II)

Guidance literature:: In dichloromethane; byproducts: cyclooctadiene; under Ar; ligand dissolved in CH2Cl2; added over 5 min to soln. of Pt complex (molar ratio 2.5:1) in CH2Cl2; stirred at room temp. for 18 h; evapd. under reduced pressure; triturated with pentane;
DOI:10.1021/om200999n