2-methyl-4-trimethylsilylbenzaldehyde ethylene acetal

Base Information

Chemical Name:2-methyl-4-trimethylsilylbenzaldehyde ethylene acetal
CAS No.:371785-37-4
Molecular Formula:C₁₃H₂₀O₂Si
Molecular Weight:236.386
Hs Code.:

Synonyms:2-methyl-4-trimethylsilylbenzaldehyde ethylene acetal

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Chemical Property of 2-methyl-4-trimethylsilylbenzaldehyde ethylene acetal

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Technology Process of 2-methyl-4-trimethylsilylbenzaldehyde ethylene acetal

There total 2 articles about 2-methyl-4-trimethylsilylbenzaldehyde ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1450-14-2
1,1,1,2,2,2-hexamethyldisilane

: 371785-35-2
4-chloro-2-methylbenzaldehyde ethylene acetal

: 371785-37-4
2-methyl-4-trimethylsilylbenzaldehyde ethylene acetal

Guidance literature:: With sodium methylate; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 20 ℃; for 6h;
DOI:10.3987/COM-01-9271

Reference yield:

: 40137-29-9
2-methyl-4-chlorobenzaldehyde

: 371785-37-4
2-methyl-4-trimethylsilylbenzaldehyde ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / pTSA / benzene / 12 h / 150 °C

2: 78 percent / NaOMe / hexamethylphosphoric acid triamide / 6 h / 20 °C

With sodium methylate; toluene-4-sulfonic acid; In N,N,N,N,N,N-hexamethylphosphoric triamide; benzene;
DOI:10.3987/COM-01-9271