tert-butyl-dimethoxy-phenylsilane

Base Information

• Chemical Name: tert-butyl-dimethoxy-phenylsilane
• CAS No.: 1015-10-7
• Molecular Formula: C₁₂H₂₀O₂Si
• Molecular Weight: 224.375
• Mol file: 1015-10-7.mol

Synonyms:tert-butyl-dimethoxy-phenylsilane

Chemical Property of tert-butyl-dimethoxy-phenylsilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tert-butyl-dimethoxy-phenylsilane

There total 3 articles about tert-butyl-dimethoxy-phenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

methanol (67-56-1) + phenyl-tert-butyldichlorosilane (17887-41-1) → tert-butyl-dimethoxy-phenylsilane (1015-10-7)

Guidance literature:

With dmap; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja805848z

Reference yield:

Phenyltrichlorosilane (98-13-5) → tert-butyl-dimethoxy-phenylsilane (1015-10-7)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 0 °C

2: PhSiCl₃, 2,2,5-trimethyl-hexane / 110 °C

With 2,2,5-trimethylhexane; Phenyltrichlorosilane; In benzene;

DOI:10.1021/jo01051a069

Reference yield:

tertiary butyl chloride (507-20-0) + phenyl trimethylsiloxane (2996-92-1,46143-12-8) → tert-butyl-dimethoxy-phenylsilane (1015-10-7)

Guidance literature:

With 2,2,5-trimethylhexane; Phenyltrichlorosilane; at 110 ℃;

DOI:10.1021/jo01051a069

upstream raw materials:

tertiary butyl chloride

phenyl trimethylsiloxane

Phenyltrichlorosilane

methanol

Downstream raw materials:

n-butyl-tert-butyl-methoxy-phenylsilane