(E)-5-methoxy-3-(3-methoxy-3-oxoprop-1-en-1-yl)-2-(methylcarbamoyl)phenyl 4-chlorobenzoate

Base Information

Chemical Name:(E)-5-methoxy-3-(3-methoxy-3-oxoprop-1-en-1-yl)-2-(methylcarbamoyl)phenyl 4-chlorobenzoate
CAS No.:1613320-08-3
Molecular Formula:C₂₀H₁₈ClNO₆
Molecular Weight:403.819
Hs Code.:

Synonyms:(E)-5-methoxy-3-(3-methoxy-3-oxoprop-1-en-1-yl)-2-(methylcarbamoyl)phenyl 4-chlorobenzoate

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Chemical Property of (E)-5-methoxy-3-(3-methoxy-3-oxoprop-1-en-1-yl)-2-(methylcarbamoyl)phenyl 4-chlorobenzoate

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Technology Process of (E)-5-methoxy-3-(3-methoxy-3-oxoprop-1-en-1-yl)-2-(methylcarbamoyl)phenyl 4-chlorobenzoate

There total 2 articles about (E)-5-methoxy-3-(3-methoxy-3-oxoprop-1-en-1-yl)-2-(methylcarbamoyl)phenyl 4-chlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1613319-90-6
5-methoxy-2-(methylcarbamoyl)phenyl 4-chlorobenzoate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1613320-08-3
(E)-5-methoxy-3-(3-methoxy-3-oxoprop-1-en-1-yl)-2-(methylcarbamoyl)phenyl 4-chlorobenzoate

Guidance literature:: With potassium hexafluorophosphate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper(II) acetate monohydrate; In water; at 100 ℃; for 24h;
DOI:10.1002/chem.201304646

Reference yield:

: 74-11-3
para-chlorobenzoic acid

: 3400-22-4
4-methoxy-N-methylbenzamide

: 1613320-08-3
(E)-5-methoxy-3-(3-methoxy-3-oxoprop-1-en-1-yl)-2-(methylcarbamoyl)phenyl 4-chlorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; silver hexafluoroantimonate; ammonium peroxydisulfate / 1,2-dichloro-ethane / 24 h / 100 °C / Inert atmosphere

2: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; potassium hexafluorophosphate; copper(II) acetate monohydrate / water / 24 h / 100 °C

With potassium hexafluorophosphate; ammonium peroxydisulfate; silver hexafluoroantimonate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper(II) acetate monohydrate; In water; 1,2-dichloro-ethane;
DOI:10.1002/chem.201304646