4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester

Base Information

• Chemical Name: 4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester
• CAS No.: 134266-21-0
• Molecular Formula: C₁₅H₁₇IN₂O₅
• Molecular Weight: 432.215

Synonyms:4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester

Chemical Property of 4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester

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Technology Process of 4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester

There total 1 articles about 4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

5-iodovaniline (5438-36-8) + ethyl acetoacetate (141-97-9) + urea (57-13-6) → 4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester (134266-21-0)

Guidance literature:

hydrogenchloride; In ethanol; for 3h; Heating;

Reference yield: 83.0%

4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester (134266-21-0) → 4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid hydrazide (134266-28-7)

Guidance literature:

With hydrazine; In ethanol; for 3h; Heating;

Reference yield: 82.0%

4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester (134266-21-0) + phenylhydrazine (100-63-0) → 4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid N'-phenyl-hydrazide (134266-29-8)

Guidance literature:

With hydrazine; In ethanol; for 3h; Heating;

upstream raw materials:

5-iodovaniline

ethyl acetoacetate

urea

Downstream raw materials:

Benzoic acid N'-[4-(4-hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carbonyl]-hydrazide

4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid hydrazide

4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid N'-phenyl-hydrazide

4-(4-Hydroxy-3-iodo-5-methoxy-phenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid N'-(2,4-dinitro-phenyl)-hydrazide

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