pentyl 2-oxo-2-phenylacetate

Base Information

• Chemical Name: pentyl 2-oxo-2-phenylacetate
• CAS No.: 31197-64-5
• Molecular Formula: C₁₃H₁₆O₃
• Molecular Weight: 220.268
• Mol file: 31197-64-5.mol

Synonyms:pentyl 2-oxo-2-phenylacetate

Chemical Property of pentyl 2-oxo-2-phenylacetate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of pentyl 2-oxo-2-phenylacetate

There total 10 articles about pentyl 2-oxo-2-phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

pentan-1-ol (71-41-0) + 4,4,4-trifluoro-3-hydroxy-1-phenylbut-2-en-1-one (41463-86-9) → pentyl 2-oxo-2-phenylacetate (31197-64-5)

Guidance literature:

With tert.-butylhydroperoxide; iodine; sodium carbonate; In 1,2-dichloro-ethane; at 60 ℃; for 7h;

DOI:10.1055/s-0036-1588833

Reference yield: 80.0%

α-hydroxyphenylacetic acid pentyl ester (20309-57-3) → pentyl 2-oxo-2-phenylacetate (31197-64-5)

Guidance literature:

With aluminum oxide; ammonium chloroformate; In cyclohexane; at 60 ℃; for 13.5h;

DOI:10.1080/00397919908085939

Reference yield: 78.0%

potassium amylxanthate (2720-73-2) + acetophenone (98-86-2) → pentyl 2-oxo-2-phenylacetate (31197-64-5)

Guidance literature:

With iodine; dimethyl sulfoxide; In water; at 80 ℃; for 12h; Schlenk technique;

DOI:10.1021/acs.joc.9b03272

upstream raw materials:

α-hydroxyphenylacetic acid pentyl ester

pentan-1-ol

Benzoylformic acid

MANDELIC ACID