methyl 5-(4-iodophenyl)pentanoate

Base Information

Chemical Name:methyl 5-(4-iodophenyl)pentanoate
CAS No.:408316-46-1
Molecular Formula:C₁₂H₁₅IO₂
Molecular Weight:318.154
Hs Code.:

Synonyms:methyl 5-(4-iodophenyl)pentanoate

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Chemical Property of methyl 5-(4-iodophenyl)pentanoate

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Technology Process of methyl 5-(4-iodophenyl)pentanoate

There total 3 articles about methyl 5-(4-iodophenyl)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 67-56-1
methanol

: 116680-98-9
5-(4-iodophenyl)pentanoic acid

: 408316-46-1
methyl 5-(4-iodophenyl)pentanoate

Guidance literature:: methanol; With acetyl chloride; at 0 ℃; for 0.166667h; Inert atmosphere;

5-(4-iodophenyl)pentanoic acid; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.3390/molecules25040769

Reference yield: 93.0%

: 20620-59-1
5-phenyl-n-valeric acid methyl ester

: 408316-46-1
methyl 5-(4-iodophenyl)pentanoate

Guidance literature:: 5-phenyl-n-valeric acid methyl ester; With thallium(III) trifluoroacetate; In trifluoroacetic acid; at 20 ℃; for 120h;

With potassium iodide; In water; trifluoroacetic acid; for 0.25h;
DOI:10.1016/S0040-4020(01)01048-1

Reference yield:

: 2270-20-4
5-Phenylpentanoic acid

: 408316-46-1
methyl 5-(4-iodophenyl)pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / H₅IO₆; I₂; aq. H₂SO₄ / acetic acid / 18 h / 75 °C

2: 97 percent / H₂SO₄ / 21 h / Heating

With sulfuric acid; iodine; periodic acid; In acetic acid;
DOI:10.1016/j.tet.2004.05.062