3-(5,6-Dimethyl-1h-benzo[d]imidazol-2-ylamino)propan-1-ol

Base Information

Chemical Name:3-(5,6-Dimethyl-1h-benzo[d]imidazol-2-ylamino)propan-1-ol
CAS No.:301163-47-3
Molecular Formula:C₁₂H₁₇N₃O
Molecular Weight:219.286
Hs Code.:
DSSTox Substance ID:DTXSID201207245

Synonyms:301163-47-3;3-(5,6-dimethyl-1h-benzo[d]imidazol-2-ylamino)propan-1-ol;3-[(5,6-dimethyl-1H-benzimidazol-2-yl)amino]propan-1-ol;1-Propanol, 3-[(5,6-dimethyl-1H-benzimidazol-2-yl)amino]-;SCHEMBL1059363;DTXSID201207245;CCG-104731;EU-0035642;SR-01000318117;SR-01000318117-1;3-[(5,6-Dimethyl-1H-benzimidazol-2-yl)amino]-1-propanol

Suppliers and Price of 3-(5,6-Dimethyl-1h-benzo[d]imidazol-2-ylamino)propan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
3-(5,6-Dimethyl-1H-benzo[d]imidazol-2-ylamino)propan-1-ol 95%
25g
$ 4070.00

Matrix Scientific
3-(5,6-Dimethyl-1H-benzo[d]imidazol-2-ylamino)propan-1-ol 95%
5g
$ 1518.00

Total 2 raw suppliers

Chemical Property of 3-(5,6-Dimethyl-1h-benzo[d]imidazol-2-ylamino)propan-1-ol

Chemical Property:

Boiling Point:447.5±47.0 °C(Predicted)
Density:1.234±0.06 g/cm3(Predicted)
XLogP3:2.8
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:219.137162174
Heavy Atom Count:16
Complexity:224

Purity/Quality:

95%-98% ^*data from raw suppliers

3-(5,6-Dimethyl-1H-benzo[d]imidazol-2-ylamino)propan-1-ol 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC2=C(C=C1C)N=C(N2)NCCCO

Technology Process of 3-(5,6-Dimethyl-1h-benzo[d]imidazol-2-ylamino)propan-1-ol

There total 3 articles about 3-(5,6-Dimethyl-1h-benzo[d]imidazol-2-ylamino)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1189164-12-2
2-bromo-5,6-dimethyl-1H-benzo[d]imidazole

: 156-87-6
propan-1-ol-3-amine

: 301163-47-3
3-((5,6-dimethyl-1H-benzo[d]imidazol-2-yl)amino)propan-1-ol

Guidance literature:: at 180 ℃; for 0.5h; Microwave irradiation;
DOI:10.1021/jm1000248

Reference yield:

: 3287-79-4
5,6-dimethyl-2-mercaptobenzimidazole

: 301163-47-3
3-((5,6-dimethyl-1H-benzo[d]imidazol-2-yl)amino)propan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide; bromine; acetic acid / water / 4.5 h / 0 - 23 °C

2: 0.5 h / 180 °C / Microwave irradiation

With hydrogen bromide; bromine; acetic acid; In water;
DOI:10.3762/bjoc.9.103

Reference yield:

: 3171-45-7
4,5-dimethyl-1,2-phenylenediamine

: 301163-47-3
3-((5,6-dimethyl-1H-benzo[d]imidazol-2-yl)amino)propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol; water / 3 h / Reflux

2: hydrogen bromide; bromine; acetic acid / water / 4.5 h / 0 - 23 °C

3: 0.5 h / 180 °C / Microwave irradiation

With hydrogen bromide; bromine; acetic acid; In ethanol; water;
DOI:10.3762/bjoc.9.103