Difluoro[2,4,6-tris(1-methylethyl)phenyl]borane

Base Information

Chemical Name:Difluoro[2,4,6-tris(1-methylethyl)phenyl]borane
CAS No.:215102-78-6
Molecular Formula:C₁₅H₂₃BF₂
Molecular Weight:252.155
Hs Code.:
DSSTox Substance ID:DTXSID701243511

Synonyms:Difluoro[2,4,6-tris(1-methylethyl)phenyl]borane;DTXSID701243511;215102-78-6

Suppliers and Price of Difluoro[2,4,6-tris(1-methylethyl)phenyl]borane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Difluoro[2,4,6-tris(1-methylethyl)phenyl]borane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:252.1860872
Heavy Atom Count:18
Complexity:233

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B(C1=C(C=C(C=C1C(C)C)C(C)C)C(C)C)(F)F

Technology Process of Difluoro[2,4,6-tris(1-methylethyl)phenyl]borane

There total 1 articles about Difluoro[2,4,6-tris(1-methylethyl)phenyl]borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 215102-95-7
dichloro(2,4,6-triisopropylphenyl)borane

: 7681-49-4
sodium fluoride

: 215102-78-6
difluoro(2,4,6-triisopropylphenyl)borane

Guidance literature:: In acetonitrile; N2 atm.; molar ratio Cl2BR:NaF 1:5, refluxing (3 h); evapn., distn. (0.01 mbar); elem. anal.;

Reference yield: 91.0%

: 215102-78-6
difluoro(2,4,6-triisopropylphenyl)borane

: 74-89-5
methylamine

: 215102-80-0
bis(methylamino)-(2,4,6-triisopropylphenyl)borane

Guidance literature:: With BuLi; In hexane; byproducts: LiF; N2 atm.; molar ratio RNH2:BuLi:F2BR 3:2:1, cooling (-30°C), heating (20°C), stirring (0°C), refluxing (2 h); evapn., distn. (vac.); elem. anal.;

Reference yield: 90.0%

: 215102-78-6
difluoro(2,4,6-triisopropylphenyl)borane

: 75-64-9
tert-butylamine

: 215102-85-5
bis(tert-butyl)-(2,4,6-triisopropylphenyl)borane

Guidance literature:: With BuLi; In hexane; byproducts: LiF; N2 atm.; equimolar ratio RNH2:BuLi, mixing (20°C), refluxing (3 h); evapn. (vac.), distn. (vac.); elem. anal.;