2-hydroxy-2-(4-hydroxy-3-methoxy-phenyl)-acetoacetic acid ethyl ester

Base Information

• Chemical Name: 2-hydroxy-2-(4-hydroxy-3-methoxy-phenyl)-acetoacetic acid ethyl ester
• CAS No.: 860752-27-8
• Molecular Formula: C₁₃H₁₆O₆
• Molecular Weight: 268.266
• Mol file: 860752-27-8.mol

Synonyms:2-hydroxy-2-(4-hydroxy-3-methoxy-phenyl)-acetoacetic acid ethyl ester

Chemical Property of 2-hydroxy-2-(4-hydroxy-3-methoxy-phenyl)-acetoacetic acid ethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 2-hydroxy-2-(4-hydroxy-3-methoxy-phenyl)-acetoacetic acid ethyl ester

There total 1 articles about 2-hydroxy-2-(4-hydroxy-3-methoxy-phenyl)-acetoacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 2,3-dioxobutyrate (1723-25-7) + 2-methoxy-phenol (90-05-1) → 2-hydroxy-2-(4-hydroxy-3-methoxy-phenyl)-acetoacetic acid ethyl ester (860752-27-8)

Guidance literature:

With acetic acid; zinc(II) chloride;

Reference yield:

2-hydroxy-2-(4-hydroxy-3-methoxy-phenyl)-acetoacetic acid ethyl ester (860752-27-8) → (4-hydroxy-3-methoxy-phenyl)-glyoxylic acid (2021-40-1)

Guidance literature:

With water; copper (I) acetate;

Reference yield:

2-hydroxy-2-(4-hydroxy-3-methoxy-phenyl)-acetoacetic acid ethyl ester (860752-27-8) + copper diacetate (142-71-2) → (4-hydroxy-3-methoxy-phenyl)-glyoxylic acid (2021-40-1)

Guidance literature:

upstream raw materials:

ethyl 2,3-dioxobutyrate

2-methoxy-phenol

Downstream raw materials:

(4-hydroxy-3-methoxy-phenyl)-glyoxylic acid