4,5-bis(2,6-dimesitylanilino)-2,7-di-tert-butyl-9,9-dimethylxanthene

Base Information

• Chemical Name: 4,5-bis(2,6-dimesitylanilino)-2,7-di-tert-butyl-9,9-dimethylxanthene
• CAS No.: 1446716-95-5
• Molecular Formula: C₇₁H₈₀N₂O
• Molecular Weight: 977.429
• Mol file: 1446716-95-5.mol

Synonyms:4,5-bis(2,6-dimesitylanilino)-2,7-di-tert-butyl-9,9-dimethylxanthene

Chemical Property of 4,5-bis(2,6-dimesitylanilino)-2,7-di-tert-butyl-9,9-dimethylxanthene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,5-bis(2,6-dimesitylanilino)-2,7-di-tert-butyl-9,9-dimethylxanthene

There total 1 articles about 4,5-bis(2,6-dimesitylanilino)-2,7-di-tert-butyl-9,9-dimethylxanthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

2,6-bis-(2,4,6-trimethylphenyl)aniline (477933-80-5) + 4,5-dibromo-2,7-di-tert-butyl-9,9-dimethyl-9H-xanthene (130525-43-8) → 4,5-bis(2,6-dimesitylanilino)-2,7-di-tert-butyl-9,9-dimethylxanthene (1446716-95-5)

Guidance literature:

With palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; In toluene; at 95 ℃; for 72h;

DOI:10.1002/anie.201207962

Reference yield: 46.0%

hexane (110-54-3) + 4,5-bis(2,6-dimesitylanilino)-2,7-di-tert-butyl-9,9-dimethylxanthene (1446716-95-5) + potassium hydride + toluene (108-88-3,15644-74-3,16713-13-6) → C71H78N2O(2-)*2K(1+)*0.9C7H8*0.6C6H14

Guidance literature:

4,5-bis(2,6-dimesitylanilino)-2,7-di-tert-butyl-9,9-dimethylxanthene; potassium hydride; toluene; In toluene; mineral oil; at 80 ℃; for 144h;

hexane; Sonication;

DOI:10.1002/anie.201207962

Reference yield: 41.0%

Hexamethyldisiloxane (107-46-0) + 4,5-bis(2,6-dimesitylanilino)-2,7-di-tert-butyl-9,9-dimethylxanthene (1446716-95-5) + potassium hydride → C71H78N2O(2-)*2K(1+)

Guidance literature:

4,5-bis(2,6-dimesitylanilino)-2,7-di-tert-butyl-9,9-dimethylxanthene; potassium hydride; In toluene; mineral oil; at 80 ℃; for 144h;

Hexamethyldisiloxane; Sonication;

DOI:10.1002/anie.201207962

upstream raw materials:

2,6-bis-(2,4,6-trimethylphenyl)aniline

4,5-dibromo-2,7-di-tert-butyl-9,9-dimethyl-9H-xanthene

Refernces