(2S)-2-{[(2S)-2-{[(2S)-2-{[(4-{[(2,6-dimethylphenyl)carbamoyl]amino}phenyl)acetyl]amino}-4-methylpentanoyl]amino}-4-methoxy-4-oxobutanoyl]amino}-3-methylbutanoic acid

Base Information

Chemical Name:(2S)-2-{[(2S)-2-{[(2S)-2-{[(4-{[(2,6-dimethylphenyl)carbamoyl]amino}phenyl)acetyl]amino}-4-methylpentanoyl]amino}-4-methoxy-4-oxobutanoyl]amino}-3-methylbutanoic acid
CAS No.:1355027-72-3
Molecular Formula:C₃₃H₄₅N₅O₈
Molecular Weight:639.749
Hs Code.:

(2S)-2-{[(2S)-2-{[(2S)-2-{[(4-{[(2,6-dimethylphenyl)carbamoyl]amino}phenyl)acetyl]amino}-4-methylpentanoyl]amino}-4-methoxy-4-oxobutanoyl]amino}-3-methylbutanoic acid

Synonyms:(2S)-2-{[(2S)-2-{[(2S)-2-{[(4-{[(2,6-dimethylphenyl)carbamoyl]amino}phenyl)acetyl]amino}-4-methylpentanoyl]amino}-4-methoxy-4-oxobutanoyl]amino}-3-methylbutanoic acid

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Chemical Property of (2S)-2-{[(2S)-2-{[(2S)-2-{[(4-{[(2,6-dimethylphenyl)carbamoyl]amino}phenyl)acetyl]amino}-4-methylpentanoyl]amino}-4-methoxy-4-oxobutanoyl]amino}-3-methylbutanoic acid

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Technology Process of (2S)-2-{[(2S)-2-{[(2S)-2-{[(4-{[(2,6-dimethylphenyl)carbamoyl]amino}phenyl)acetyl]amino}-4-methylpentanoyl]amino}-4-methoxy-4-oxobutanoyl]amino}-3-methylbutanoic acid

There total 10 articles about (2S)-2-{[(2S)-2-{[(2S)-2-{[(4-{[(2,6-dimethylphenyl)carbamoyl]amino}phenyl)acetyl]amino}-4-methylpentanoyl]amino}-4-methoxy-4-oxobutanoyl]amino}-3-methylbutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1292797-86-4
C₂₂H₃₂N₂O₇

: 1355027-72-3
(2S)-2-{[(2S)-2-{[(2S)-2-{[(4-{[(2,6-dimethylphenyl)carbamoyl]amino}phenyl)acetyl]amino}-4-methylpentanoyl]amino}-4-methoxy-4-oxobutanoyl]amino}-3-methylbutanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: dichloromethane / 2 h

2: triethylamine / dichloromethane

3: dichloromethane / 2 h

4: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide

5: palladium 10% on activated carbon; hydrogen / ethanol; N,N-dimethyl-formamide

With palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.078

Reference yield:

: 1292797-88-6
C₂HF₃O₂*C₂₃H₃₅N₃O₆

: 1355027-72-3
(2S)-2-{[(2S)-2-{[(2S)-2-{[(4-{[(2,6-dimethylphenyl)carbamoyl]amino}phenyl)acetyl]amino}-4-methylpentanoyl]amino}-4-methoxy-4-oxobutanoyl]amino}-3-methylbutanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide

2: palladium 10% on activated carbon; hydrogen / ethanol; N,N-dimethyl-formamide

With palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.078

Reference yield:

: 1292797-89-7
C₂₈H₄₃N₃O₈

: 1355027-72-3
(2S)-2-{[(2S)-2-{[(2S)-2-{[(4-{[(2,6-dimethylphenyl)carbamoyl]amino}phenyl)acetyl]amino}-4-methylpentanoyl]amino}-4-methoxy-4-oxobutanoyl]amino}-3-methylbutanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 2 h

2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide

3: palladium 10% on activated carbon; hydrogen / ethanol; N,N-dimethyl-formamide

With palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.078