2(S)-cyclohexyl-1-<((1R,2S,5R)-8-phenylmenthoxy)carbonyl>-5-(triisopropylsilyl)-2,3-dihydro-4-pyridone

Base Information

Chemical Name:2(S)-cyclohexyl-1-<((1R,2S,5R)-8-phenylmenthoxy)carbonyl>-5-(triisopropylsilyl)-2,3-dihydro-4-pyridone
CAS No.:126378-71-0
Molecular Formula:C₃₇H₅₉NO₃Si
Molecular Weight:593.966
Hs Code.:

Synonyms:2(S)-cyclohexyl-1-<((1R,2S,5R)-8-phenylmenthoxy)carbonyl>-5-(triisopropylsilyl)-2,3-dihydro-4-pyridone

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Chemical Property of 2(S)-cyclohexyl-1-<((1R,2S,5R)-8-phenylmenthoxy)carbonyl>-5-(triisopropylsilyl)-2,3-dihydro-4-pyridone

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Technology Process of 2(S)-cyclohexyl-1-<((1R,2S,5R)-8-phenylmenthoxy)carbonyl>-5-(triisopropylsilyl)-2,3-dihydro-4-pyridone

There total 7 articles about 2(S)-cyclohexyl-1-<((1R,2S,5R)-8-phenylmenthoxy)carbonyl>-5-(triisopropylsilyl)-2,3-dihydro-4-pyridone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 144375-66-6
4-Methoxy-1-[(1S,2R,5S)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyloxycarbonyl]-3-triisopropylsilanyl-pyridinium; chloride

: 931-50-0
cyclohexylmagnesium bromide

: 126378-71-0,126378-72-1
(R)-2-Cyclohexyl-4-oxo-5-triisopropylsilanyl-3,4-dihydro-2H-pyridine-1-carboxylic acid (1S,2R,5S)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:: In tetrahydrofuran; toluene; at -78 ℃; Yield given. Yields of byproduct given;
DOI:10.1021/jo00296a006

Reference yield:

: 126378-42-5
4-methoxy-3-(trisopropylsilyl)pyridine

: 126378-43-6
(1R,2S,5R)-(-)-8-phenylmenthyl chloroformate

: 931-50-0
cyclohexylmagnesium bromide

: 126378-71-0
2(S)-cyclohexyl-1-<((1R,2S,5R)-8-phenylmenthoxy)carbonyl>-5-(triisopropylsilyl)-2,3-dihydro-4-pyridone

: 2(R)-cyclohexyl-1-<((1R,2S,5R)-8-phenylmenthoxy)carbonyl>-5-(triisopropylsilyl)-2,3-dihydro-4-pyridone

Guidance literature:: Yield given. Multistep reaction. Yields of byproduct given; 1.) toluene, -23 deg C, 15 min, 2.) toluene, THF, -78 deg C, 1 h;
DOI:10.1021/ja00090a019