Methyl 5-O-Acetyl-(-)-shikimate

Base Information

Chemical Name:Methyl 5-O-Acetyl-(-)-shikimate
CAS No.:76947-24-5
Molecular Formula:C₁₀H₁₄O₆
Molecular Weight:230.218
Hs Code.:

Synonyms:Methyl 5-O-Acetyl-(-)-shikimate

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Chemical Property of Methyl 5-O-Acetyl-(-)-shikimate

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Technology Process of Methyl 5-O-Acetyl-(-)-shikimate

There total 6 articles about Methyl 5-O-Acetyl-(-)-shikimate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 143308-74-1
(3aR,7R,7aS)-methyl 7-acetoxy-2,2-dimethyl-3a,6,7,7atetrahydrobenzo[d][1,3]dioxole-5-carboxylate

: 76947-24-5
Methyl 5-O-Acetyl-(-)-shikimate

Guidance literature:: With acetic acid; In tetrahydrofuran; at 70 ℃; for 6h;
DOI:10.1021/jo00047a049

Reference yield:

: 138-59-0
shikimic acid

: 76947-24-5
Methyl 5-O-Acetyl-(-)-shikimate

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / Amberlite IR 120 / 12 h / Heating

2: 96 percent / camphorsulfonic acid / 0.25 h / Ambient temperature

3: 100 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 2 h / Ambient temperature

4: 94 percent / aq. HOAc / tetrahydrofuran / 6 h / 70 °C

With dmap; Amberlite IR 120; acetic acid; camphor-10-sulfonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00047a049

Reference yield:

: 40983-58-2
methyl shikimate

: 76947-24-5
Methyl 5-O-Acetyl-(-)-shikimate

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / camphorsulfonic acid / 0.25 h / Ambient temperature

2: 100 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 2 h / Ambient temperature

3: 94 percent / aq. HOAc / tetrahydrofuran / 6 h / 70 °C

With dmap; acetic acid; camphor-10-sulfonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00047a049