4,4,4-TRIFLUORO-1-PHENYL-2-(PHENYLHYDRAZONO)BUTANE-1,3-DIONE

Base Information

Chemical Name:4,4,4-TRIFLUORO-1-PHENYL-2-(PHENYLHYDRAZONO)BUTANE-1,3-DIONE
CAS No.:76073-64-8
Molecular Formula:C16H11 F3 N2 O2
Molecular Weight:320.27
Hs Code.:2928000090
Mol file:76073-64-8.mol

Synonyms:1,2,3-Butanetrione,4,4,4-trifluoro-1-phenyl-, 2-(phenylhydrazone) (9CI)

Suppliers and Price of 4,4,4-TRIFLUORO-1-PHENYL-2-(PHENYLHYDRAZONO)BUTANE-1,3-DIONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4,4,4-TRIFLUORO-1-PHENYL-2-(PHENYLHYDRAZONO)BUTANE-1,3-DIONE 95.00%
5MG
$ 502.59

Total 6 raw suppliers

Chemical Property of 4,4,4-TRIFLUORO-1-PHENYL-2-(PHENYLHYDRAZONO)BUTANE-1,3-DIONE

Chemical Property:

PSA：58.53000
LogP:3.54180

Purity/Quality:

99% ^*data from raw suppliers

4,4,4-TRIFLUORO-1-PHENYL-2-(PHENYLHYDRAZONO)BUTANE-1,3-DIONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4,4,4-TRIFLUORO-1-PHENYL-2-(PHENYLHYDRAZONO)BUTANE-1,3-DIONE

There total 1 articles about 4,4,4-TRIFLUORO-1-PHENYL-2-(PHENYLHYDRAZONO)BUTANE-1,3-DIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 326-06-7
1-Phenyl-4,4,4-trifluorobutane-1,3-dione

: 100-34-5
benzene diazonium chloride

: 76073-64-8
4,4,4-trifluoro-1-phenyl-1,2,3-butanetrione-2-(phenylhydrazone)

Guidance literature:: With sodium acetate; In ethanol; for 1h;
DOI:10.1007/BF00950584

Reference yield: 95.0%

: 76073-64-8
4,4,4-trifluoro-1-phenyl-1,2,3-butanetrione-2-(phenylhydrazone)

: 100-63-0
phenylhydrazine

: 76073-65-9
1,3-diphenyl-4-phenylazo-5-trifluoromethylpyrazole

Guidance literature:: In ethanol; at 20 ℃; for 1h;
DOI:10.1007/BF00950584

Reference yield:

: 142-71-2
copper diacetate

: 76073-64-8
4,4,4-trifluoro-1-phenyl-1,2,3-butanetrione-2-(phenylhydrazone)

: {N,N'-ethylenebis{4,4,4-trifluoro-1-phenyl-1,2,3-butanetrione-2-(phenylhydrazone)-1-iminato}}copper

Guidance literature:: With ethylenediamine; In ethanol; addn. of amine to suspension of ketone and Cu(OAc)2, boiling 30 min. with stirring; cooling, pptn., filtration, crystn. (CHCl3-EtOH 1:2);