[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germane

Base Information

Chemical Name:[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germane
CAS No.:162088-73-5
Molecular Formula:C₄₂H₈₄GeSi₆
Molecular Weight:830.232
Hs Code.:

Synonyms:[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germane

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Chemical Property of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germane

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Technology Process of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germane

There total 2 articles about [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 16853-85-3
lithium aluminium tetrahydride

: 162088-71-3
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)bromochloro(2,4,6-triisopropylphenyl)germane

: 162088-73-5
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germane

Guidance literature:: With NH₄Cl; In tetrahydrofuran; water; Ar-atmosphere; refluxing (10 h), NH4Cl soln. (aq) addn.; washing (HCl soln.), extg. (CHCl3), drying (MgSO4), evapn. (reduced pressure), repptn. (CH2Cl2 / EtOH, room temp.); elem. anal.;
DOI:10.1021/om00002a055

Reference yield:

: 115160-05-9
1-bromo-2,4,6-tris[bis(trimethylsilyl)methyl]benzene

: 162088-73-5
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germane

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuLi; NH₄Cl / tetrahydrofuran; pentane

2: NH₄Cl / tetrahydrofuran; water

With t-BuLi; NH₄Cl; In tetrahydrofuran; water; pentane;
DOI:10.1021/om00002a055

Reference yield: 88.0%

: 128-08-5
N-Bromosuccinimide

: 162088-73-5
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germane

: 162088-75-7
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

Guidance literature:: In benzene; Ar-atmosphere; stirring (room temp., 10 h); chromy. (SiO2, C6H6), repptn. (CHCl3 / EtOH, room temp.); elem. anal.;
DOI:10.1021/om00002a055