1-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-1-(2,4,6-triisopropylphenyl)-3,4-dimethyl-1-germa-3-cyclopentene

Base Information

Chemical Name:1-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-1-(2,4,6-triisopropylphenyl)-3,4-dimethyl-1-germa-3-cyclopentene
CAS No.:153289-22-6
Molecular Formula:C₄₈H₉₂GeSi₆
Molecular Weight:910.361
Hs Code.:

Synonyms:1-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-1-(2,4,6-triisopropylphenyl)-3,4-dimethyl-1-germa-3-cyclopentene

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Chemical Property of 1-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-1-(2,4,6-triisopropylphenyl)-3,4-dimethyl-1-germa-3-cyclopentene

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Technology Process of 1-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-1-(2,4,6-triisopropylphenyl)-3,4-dimethyl-1-germa-3-cyclopentene

There total 5 articles about 1-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-1-(2,4,6-triisopropylphenyl)-3,4-dimethyl-1-germa-3-cyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 152291-69-5
{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}(2,4,6-triisopropylphenyl)germylene

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 153289-22-6
1-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-1-(2,4,6-triisopropylphenyl)-3,4-dimethyl-1-germa-3-cyclopentene

Guidance literature:: room temp., stiring (1 h); chromatography (SiO2, hexane);
DOI:10.1021/ja991147x

Reference yield: 68.0%

: 162088-75-7
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 153289-22-6
1-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-1-(2,4,6-triisopropylphenyl)-3,4-dimethyl-1-germa-3-cyclopentene

Guidance literature:: With lithium naphthalenide; In tetrahydrofuran;
DOI:10.1039/c39950001425

Reference yield:

: 162088-75-7
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

: 153289-22-6
1-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-1-(2,4,6-triisopropylphenyl)-3,4-dimethyl-1-germa-3-cyclopentene

Guidance literature:: Multi-step reaction with 2 steps

1: LiC₁₀H₈ / tetrahydrofuran

With LiC₁₀H₈; In tetrahydrofuran;
DOI:10.1021/ja991147x