Technology Process of Copper, [2,9,16,23-tetrachloro-29H,31H-phthalocyaninato(2-)-kappaN29,kappaN30,kappaN31,kappaN32]-, (SP-4-1)-
There total 1 articles about Copper, [2,9,16,23-tetrachloro-29H,31H-phthalocyaninato(2-)-kappaN29,kappaN30,kappaN31,kappaN32]-, (SP-4-1)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
further solvent(s);
stirring of a mixt. of CuCl, urea and C8H3ClO3 in trichlorobenzene at ambient temp. for 30 minutes; heating at 175-180°C for 4 h; evapn.; heating with 5% HCl; heating with 2% aq. Na2CO3;; washing with H2O and ethanol; drying at 95-100°C;;