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2,3,4,5-Tetramethoxybenzoylchlorid

Base Information Edit
  • Chemical Name:2,3,4,5-Tetramethoxybenzoylchlorid
  • CAS No.:55386-54-4
  • Molecular Formula:C11H13ClO5
  • Molecular Weight:260.674
  • Hs Code.:
  • Mol file:55386-54-4.mol
2,3,4,5-Tetramethoxybenzoylchlorid

Synonyms:2,3,4,5-Tetramethoxybenzoylchlorid

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Chemical Property of 2,3,4,5-Tetramethoxybenzoylchlorid Edit
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Technology Process of 2,3,4,5-Tetramethoxybenzoylchlorid

There total 3 articles about 2,3,4,5-Tetramethoxybenzoylchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 ℃; for 144h; Inert atmosphere;
DOI:10.1021/np200095q
Guidance literature:
Multi-step reaction with 2 steps
1: 90 percent / Cu powder / methanol / 18 h / Heating
2: oxalyl chloride / CH2Cl2 / Ambient temperature
With oxalyl dichloride; copper; In methanol; dichloromethane;
DOI:10.1021/ja00252a022
Guidance literature:
Multi-step reaction with 3 steps
1: 96 percent / Br2 / H2O; CHCl3 / 18 h / Heating
2: 90 percent / Cu powder / methanol / 18 h / Heating
3: oxalyl chloride / CH2Cl2 / Ambient temperature
With oxalyl dichloride; bromine; copper; In methanol; dichloromethane; chloroform; water;
DOI:10.1021/ja00252a022
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