HIr(O₂CPh)(PMe₃)₃Cl

Base Information

Chemical Name:HIr(O₂CPh)(PMe₃)₃Cl
CAS No.:148424-96-8
Molecular Formula:C₁₆H₃₃ClIrO₂P₃
Molecular Weight:578.031
Hs Code.:

HIr(O<SUB>2</SUB>CPh)(PMe<SUB>3</SUB>)<SUB>3</SUB>Cl

Synonyms:HIr(O₂CPh)(PMe₃)₃Cl

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Chemical Property of HIr(O₂CPh)(PMe₃)₃Cl

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Technology Process of HIr(O₂CPh)(PMe₃)₃Cl

There total 1 articles about HIr(O₂CPh)(PMe₃)₃Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 118494-48-7
[tris-(trimethylphosphine)(cyclooctadiene)iridium(I)]chloride

: 148424-96-8
{(CH₃)3P}3Ir(H)(O₂CC₆H₅)(Cl)

Guidance literature:: With benzoic acid; In 1,3,5-trimethyl-benzene; byproducts: COD; (N2), heated at 60°C for 23 h; concd. under reduced pressure, collected by filtration, dissolved in CH2Cl2, pptd. by addn. of pentane, filtered, stripped, washed with pentane/THF, dried under reduced pressure, elem. anal.;

Reference yield: 79.0%

: 60969-19-9
thallium(I) hexafluorophosphate

: 148424-96-8
{(CH₃)3P}3Ir(H)(O₂CC₆H₅)(Cl)

: 55172-29-7,7791-12-0
thallium chloride

: {mer-(Me3P)3(η2-benzoato)hydridoiridium(III)}(PF6)

Guidance literature:: In dichloromethane; Mixing of starting compds. (N2, drybox), addn. of CH2Cl2 to mixt., magnetical stirring of react. mixt. (N2) and heating to reflux. Soln. turns gradually light red, and after 3 h at reflux, a pinkish-white ppt. is obsd. in clear soln.; Removal of ppt. by filtn., stripping of CH2Cl2 soln. under reduced pressure, drying of resulting solid (reduced pressure), elem. anal.;