C₂₇H₃₅FN₂O₄

Base Information

Chemical Name:C₂₇H₃₅FN₂O₄
CAS No.:852660-63-0
Molecular Formula:C₂₇H₃₅FN₂O₄
Molecular Weight:470.584
Hs Code.:

C<sub>27</sub>H<sub>35</sub>FN<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₇H₃₅FN₂O₄

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Chemical Property of C₂₇H₃₅FN₂O₄

Chemical Property:

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Technology Process of C₂₇H₃₅FN₂O₄

There total 15 articles about C₂₇H₃₅FN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 459872-39-0
N-[3-(4-fluorophenyl)propyl]-N-methylamine

: 813445-36-2
{(7R,8R)-8-formyl-1,4-dioxa-spiro[4.5]dec-7-yl}-carbamic acid benzyl ester

: 852660-63-0
C₂₇H₃₅FN₂O₄

Guidance literature:: N-[3-(4-fluorophenyl)propyl]-N-methylamine; {(7R,8R)-8-formyl-1,4-dioxa-spiro[4.5]dec-7-yl}-carbamic acid benzyl ester; In dichloromethane; at 20 ℃; for 0.5h;

With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 136265-10-6,352-03-4,24393-50-8
ethyl 4-fluorocinnamate

: 852660-63-0
C₂₇H₃₅FN₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 2585.81 Torr

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 72 h / 0 - 20 °C

2.2: 1 h

3.1: phosphorus tribromide / chloroform / 25 °C / Heating / reflux

4.1: tetrahydrofuran / 25 °C

5.1: dichloromethane / 0.5 h / 20 °C

5.2: 16 h / 20 °C

With lithium aluminium tetrahydride; hydrogen; phosphorus tribromide; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; chloroform;

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 852660-63-0
C₂₇H₃₅FN₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene / Heating / reflux

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 2585.81 Torr

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 72 h / 0 - 20 °C

3.2: 1 h

4.1: phosphorus tribromide / chloroform / 25 °C / Heating / reflux

5.1: tetrahydrofuran / 25 °C

6.1: dichloromethane / 0.5 h / 20 °C

6.2: 16 h / 20 °C

With lithium aluminium tetrahydride; hydrogen; phosphorus tribromide; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; chloroform; toluene;